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GCMS analysis results for sample AE12475, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12475 conducted on June 4, 2002.

NYC-WTC_000014125–000014146

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052802\12475.D Vial: 13 Acq On : 29 May 2002 12:04 am Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 12 Anthracene, 2-methyl- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.25 ug/L 251154 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12- 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97- 59 3 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 59 4 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-/ 53 Abundance Scan 3312 (22.539 min): 12475.D (-3305) (-) m/z 192.10 100.00% 192

5000 ............................ .............. ...

146 160 40 0 ■ i" “ i Im 70 82 $6 TTprTTTJTTTTpTTnTTTTTpTnrrpnn^^ - 22.20 22.40 22.60 22.80 m/z 191.00 22.93% m/z-> 2030405060 70 8090 100110120130 140150160 170 180 190 200 Abundance #125847: Anthracene, 2-methyl- 1912

5000 22.20 22.40 22.60 22.80 " ' m/z 193.10 12.22% 28 39 51 63 82 %6 115 126 139 152 165 176 01TITmPTTTLTTTTTTTTTTTTTTIPTmTThgmt 1ap niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 2(X) Abundance #80965: 2,5-Dihydrophosphole, 3-methyH-oxo-1-phenyl- 192 164 1 ‘ i 1 ■ ■ ‘ i ' ■ TTt’I1I6F’I 22.20 22.40 22.60 22.80 5000 99 m/z 160.10 10.85% 115 47 77 177 67 125 146 04 27 36, rudjuikmerum frogeen’ rlr, 8744444434,4155, I,... . |,57 J| Tjn m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 192 22.20 22.40 22.60 22.80 m/z 146.10 10.73% 5000

89 175 — 63 117 145 45 I , , 77 105 1 7 135 1,

n/z-> 0 ----Hy ++Tprptgttu TTHT 163 20 30 40 50 60 70 80 90 100 110 120130 140 150 160 170180 190 200 I .. ..A ... 22.20 22.40 22.60 22.80 '

12475.D 052202.M Thu May 30 10:43:32 2002 Page 15

NYC-WTC_000014144

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NYC-WTC_000014144Source: NYC Law Department, mirrored locally

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