GCMS blank analysis results for sample AE06338, May 2 2002

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Library Search Compound Report

Data File C : \MSDCHEM\ 1 \DATA\ 0 5 010 2 \ 0 4 2 9LB . D Vial: 10 Acq On 1 May 2002 5:02 pm Operator: Mclean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Anthracene, 2-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 22.58 0.27 ug/L 157462 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Anthracene, 2-methyl- 192 C15H12 000613-12-7 64 2 2,5-Dihydrophosphole, 3-methyl-1... 192 C11H13OP 1000196-97-5 59 3 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 50 4 4-Hydroxy-3 ,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 45 Abundance Scan 3320 (22.586 min): 0429LB.D (-3310) (-) m/z 192.10 100.00% 192

5000 - 40 64 82 96 146 160 22.20 22.40 22.60 22.80 23.00 +49. - -L i1'111''1111 ■ ■11' ■ ‘11' ■ ■' 111 11''11 I m/Z 191.10 23 .25% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125845: Anthracene, 2-methyl- 192 A

5000 ............ 1,1 22 20 22.40 22.60 22.80 23.00 m/z 40.10 15.69% 96 165 . MWWyWAv 1 66 75 87 „| 115 126 139 152 J 1/6 । r 11 ’ I'li 1111111 j । ITTi । |*r r 11111 it । i 11 i'| 111 r |'l ’ 111 ill । [ । tri mil’l m/z-> 20 30 40 50 60 70 _80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1 -oxo-1 -phenyl- 192 164 1dt.t 1 I I ' 1 I I I ‘ t I I I I I I I I I I 22.20 22.40 22.60 22.80 23.00 5000 99 m/z 146.10 14.118 115 47 77 177 67 125,34 146 27 3?, 157 , +7+7 11341/4155, ThTTmtr 1 I1 " ’ I " 1 ‘I1 TrM. I1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester ...................... ). 192 22.20 22.40 22.60 22.80 23.00 m/z 193.10 11.26%|

5000 A

. ...................... 1 | T , TE’’’TTTTTTTTTTTTTTTTT , 90 , 108 122 134 148 160 ‘ I ' 1 1 ' 1 1 ' ( 1 1 1 ' i 1 1 1dil m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

0429LB.D 050102.M Thu May 02 14:53:46 2002 Page 8

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