GCMS calibration table data, sample AE10517, May 22, 2002

Machine-extracted title · confidence 90%

Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

NYC-WTC_000013285–000013308

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 2,5-Dihydrophosphole, 3-met... Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

22.54 0.28 ug/L 260144 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97- 59 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-/ 50 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40/9 42 4 Anthracene, 2-methyl- 192 C15H12 000613-12-7 40 Abundance Scan 3312 (22.539 min): 10517.D (-3305) (-) m/z 192.10 0.00% 192 A

5000

. 82 96 . 146 160 22.20 22.40 22.60 22.80 A 49 66 82 120 || . 0! 11 I 11 I | i | | | | i I i i'] i > i i | i > 11 J । i i 11 111 i | । 111 11 l 1 1 | i n 1 | 11 | 11 11 i r,. .'I . । |. I ।। I' 4m m/z 191.00 21.92% -n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 1912 164

5000 99 115 ■ ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ 1 ■ ■ i 22.20 22.40 22.60 22.80 47 77 177 m/z 193.10 12.82% 4457,41++8741+4+4l+4.+4155. Mt u 67' 125 146 27 3?! 0 TTWTITNTTTT n/z-> 20 30 40 50 60 70 80 90 100 110 120 130140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192 • * । ' * • * i * • I ‘ * i ‘ 1 * ‘ I 22.20 22.40 22.60 22.80 5000, m/z 95.90 11.87%

69 108 134 45 O' mTTTTTT 1 , 90 | 122 | 148 160 I...... 11144144 A mfe-> 2030405060 70 8090 100110120130140150160170180190200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- ■ ' i • ■ ■ ' i 1512 22.20 22.40 22.60 22.80 161 m/z 146.00 10.48%

5000 77 91 121 149 103 138 52 64 । mfe-> 0 ' i11" I" " I' Ju_ 11′81 Papa 2030405060 70 8090 100 110 120 130 140150 160 170 180 190 200 H Pr 0 1 I ‘ I‘ ‘ • I 22.20 22.40 22.60 22.80

10517.D 052202.M Wed May 22 11:48:17 2002 Page 11

NYC-WTC_000013298

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