GCMS calibration table data, sample AE10517, May 22, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Phenanthrene-diO Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

23.07 0.25 ug/L 236151 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 93 2 Anthracene-dlO- 188 C14D10 001719-06-8 93* 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 4 Pentacyclo[7.3.1.1.(4,12).0(2,7)♦.. 188 C14H20 1000215-61-8 38 Abundance Scan 3402 (23.068 min): 10517.D (-3396) (-) m/z 188.10 100.00% 188

5000

m/z-> 0 442,54.6,140.1122,1 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 i । 22.80 23.00 23.20 23.40 m/z 189.10 15.53% Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 m/z 184.10 14.21% 94 80 160 30 42 52 il 66 108118 132 146 1I 170179,1,1 0-TPTTTHTTTH 1mtt TTTNTTTTTTTTTTTTT ‘I m/z-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188 r i I i — Prt . 22.80 23.00 23.20 23.40 5000 m/z 80.10 12.58%

17 30 42 52 65 80 94. 160 , , , 108118 132 146 ,|.| 170179,i 0 109BWTTHTmHTt[ [ I I I, I 1 11 | ll 1 I | 1 I 11 |l|l I') I I I I | 1 1 I'I'I'l I I I | I 1 11 [Hi l I I "T m/z-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 22.80 23.00 23.20 23.40 m/z 94.05 12.52% 145 5000

117 0 41 51 63 77 89 । 159 173 I mhrtmmp102 [130

mfe-> 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10517.D 052202.M Wed May 22 11:48:19 2002 Page 12

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