GCMS calibration table data, sample AE10517, May 22, 2002

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Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

NYC-WTC_000013285–000013308

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document LLOLCLY DEdLtI toupOULC KCpOL L

Data File : C:\MSDCHEM\1\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Benzoic acid, 2-(diethylami... Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 30.94 0.21 ug/L 150896 Chrysene-dl2 30.76 Hit# of 5 Tentative ID MW MolForm CAS# Qu. 1 Benzoic acid, 2-(diethylamino)et... 221 C13H19NO2 002572-39-6 2 Phenol, 6-methyl-2-[(4-morpholin... 207 C12H17NO2 060460-71-1/ 5 3 Morpholine, 4-[(4-methylphenyl)s... 241 C11H15NO3S 006339-26 5 4 1 - [4 -Aminobenzyl ] hypoxanthine 241 C12H11N5O 1000213- -8 5 Abundance Scan 4742 (30.941 min): 10517.D (-4740) (-) m/z 207.00 100.00% 106 207 86 232 __

5000 40 -F1B5 ’ , t 14/47/1/287" 1 1 n , 30.60 30.80 31.00 31.20 Of i ■ ‘ m/z 106.20 99.06% niz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #34922: Benzoic acid, 2-(diethylamino)ethyl ester 86 105 149 5000 58 30 30.60 30.80 31.00 31.20 m/2 86.10 78.40%

miz-> 0!FTF 20 40 60 80 H100 122 1 I' ' ' 1 1 ‘ ‘ ‘ . । 176 192 206 | 120 140 160 180 200 220 240 L 221 । * Pfalput

Abundance #84739: Phenol, 6-methyl-2-I(4-morpholiny!)methyl]-

86 207 ANANAnadakdianadAug 30,60 30.80 31.0Q 31.20 5000 121 m/z 232.20 75.59% 57 | 100 176 . ... 134 149160 41 n/z-> 74. 0 1T I ■ ■ ■ • 20 40 60 i ■ hafr ■ ., ,• ■I■ i ■, •II,■ 1111190 80 100 120 140 160 180 200 220 240 Abundance #34758: Morpholine, 4-[(4-methylpheny!)sulfonyl]- 56 86 30.60 30.80 31.00 31.20 m/z 40.10 28.64% 5000 155 241 105 178 AAhul MAaMLAt 01 i ■ ■ ' 1 i ■ ■ i ■ ■ ■ ■ i ‘ 1 ■ ■ i ■ ■ ' ' i ' 1 ' ' 1 1 1 1 1 1 T T ■ l ■ ■ ■ ■ i ■ • m/z-> 20 40 60 80 100 120 140 160 180 . 200 220 240 30.60 30.80 31.00 31.20

10517.D 052202.M Wed May 22 11:48:21 2002 Page 13

NYC-WTC_000013300

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NYC-WTC_000013300Source: NYC Law Department, mirrored locally

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