GCMS analysis results for sample AE11410, May 22 2002

NYC 9/11 Public Portal Document LLOLdLY DEdrtil COILpOuU KCPOL L

Data File : C:\MSDCHEM\1\DATA\051702\11409.D Vial: 12 Acq On : 17 May 2002 9:45 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 2,2'-Binaphthalene, 1,1',2,. Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

34.91 0.25 ug/L 161350 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,2'-Binaphthalene, 1,1',2,2',3,. . 262 C20H22 027426-98-8 2 Benzene, 1,3-bis(l-buten-3-yl-)- 186 C14H18 1000159-90- 3 l,4-Methanonaphthalen-9-ol, 1,2,. . 160 C11H120 055255-94-2 4 1,4-Methanonaphthalen-9-ol, 1,2,. . 160 C11H120 001198-20-5, Abundance Scan 5417 (34.907 min): 11409.D (-5416) (-) m/z 131.50 100 131 263 5000 209 281 36 49 J _ ’ 11 ummom .'।■ । । । i । । । । । । 73 116 34.60 34.80 35.00 35.20

miz-> Abundance 0- 20 40 60 Hg i ■1111 ■' ■111 140 160 180 200 220 240 260 280 100 120 #59484:2,2'-Binaphthalene, 1,1’,2,2’,3,3’,4,4’-octahydro- ■ ■ i ■ ■ ■ ■ i'1 ■ -1 ■ ■ m/z 263.10 11 64.68%

111

5000 262 — 91 104 34.60 34.80 35.00 35.20 m/ z 2 0 9.00 45.11% o1 15। re , 391 53"’’1 । i 78th , "r , 11.। 117I1 1, ' 144157171 1 I '1 1 1111 189202215 234 i 1 1 rl i f’T" 11/47111’111’1/111+11 | 1111 miz- > 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #59061: Benzene, 1,3-bis(1-buten-3-yl-)- 55 131

34.60 34.80 35.00 35.20 5000 m/z 281.10 41.06% 91 115 29 186 77 171

m/z-> 0- .114.4 H . . r L । 1". , 144157 20 40 60 80 100 120 140 160 180 200 220 240 260 280 H , ii-iIJ| । , 1 . । " । , । ■ ! । । । । i । । । । । i, । । । । । । । । ।

Abundance #122019:1,4-Methanonaphthalen-9-ol, 1,2,3,4-tetrahydro- 131 34.60 34.80 35.00 35.20 m/z 262.10 39.15%|

5000

115 29 160 51 77 91 0 Il I i i ■ ■ i'1 ' ■ i1 1 ■ ■ i 11 -p-TT-r-p-rr-r-j- /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20

11409.D 050102.M Tue May 21 11:57:16 2002 Page 11

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