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GCMS blank analysis results for sample AE09329, May 7 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank test results for various organic compounds on May 7, 2002.

NYC-WTC_000044559–000044571

Folder label: “GCMS X 4/29/02 A 5/3/02

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NYC 9/11 Public Portal Document Llorary DedrCIi totpOuiU RCpOL

Data File C:\MSDCHEM\1\DATA\050202\0429LB.D Vial: 6 Acq On 2 May 2002 3:38 pm Operator: Mclean Sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98. L ********************************************************************* Peak Number 3 Phenanthrene, 9-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.24 ug/L 164441 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Bitoscanate 192 C8H4N2S2 004044-65-9 42 3 1H-2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 1000196-69-5 42 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 36 Abundance Scan 3319 (22.580 min): 0429LB.D (-3314) (-) m/z 192.05 100.00% 192

5000

TT \ Th ■i 1 1 96 ...... 40,7 49 70 -HH 82 | 146 160 ----- II 22.20 22.40 22.60 22.80 23.00 m/ z 96.10 17.40% ■I11" i11111" I'1111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

— 5000 1 ■ i r 1 1 1 i ' ‘ 22.20 22.40 22.60 22.80 23.00 m/ Z 191.00 17.19% 96 165 i i 29 39 51 63 74 83 j 115 126 139 152 j 176 [ | i । । 1 1 1 । 1 1 । i'| i 1 1 1 |' 1 1 I 1 । i‘i i i f n‘t' i' |' I i t'l । 1 I 'I 1 । 1 1 1 1 । 1 r 1 1 । rOTT । > T| । । । । |‘ i । । | i l । । | > ill | । । । l | I I TT6 ‘* m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125828: Bitoscanate 192

22.20 22.40 22.60 22.80 23.00 5000 m/z 146.10 16.13% 134 160 50 63 75 90 1 02 122 148 176 111,11111111111, r‘ , H# A-rl rH-rrht 1111 |'i 111111 । ■ 1 1 i■ 1 ' ........ .......... I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80945:1 H-2-lndenone,2,4,5,6,7,7a-hexahydro-3-(1-methylet... 192 ....... A 22.20 22.40 22.60 22.80 23.00 149 m/z 193.10 15.37% 177 5000 41 93 107 121 135 164 55 67 79

m/z~> ""[‘T 27 L 1160,41l4+44141llpll,+44444 1504l7HLH Her 20 30 40 50 70 80 90 100 110 120 130 140 Pi 11 rr"l 160 170 180 190 200 ’ i ' ' 1 ' l ’

22.20 22.40 22.60 22.80 23.00 '

0429LB.D 050102.M Mon May 06 10:58:31 2002 Page 6

NYC-WTC_000044567

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NYC-WTC_000044567Source: NYC Law Department, mirrored locally

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