GCMS analysis results for sample AE12474, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12474 conducted on June 4, 2002.

NYC-WTC_000014102–000014124

Folder label: “GCMS X 5/24/02 A 5/28/02”

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NYC 9/11 Public Portal Document JJLJLCLy ocaicu toupouLU KepOL L

Data File : C:\MSDCHEM\1\DATA\052802\12474.D Vial: 12 Acq On : 28 May 2002 11:15 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Phenanthrene, 9-methyl- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 22.53 0.25 ug/L 232931 Phenanthranerie-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 /53 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2/45 ■ 3 5H-Dibenzo[a,d]cycloheptene 192 C15H12 000256-81-5 45 ' 4 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 42 Abundance Scan 3311 (22.533 min): 12474.D (-3304) (-) m/z 192.10 100.00% 192

5000 ........ M.......... 70 82 96 146 160 1 22.20 22.40 22.60 22.80 1,1 m/z—> 42 51 0 TPTTTTTTIT TpHHmmmm 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.10 15.05% Abundance #81033: Phenanthrene, 9-methyl- 19/2

5000 22.20 22.40 22.60 22.80 m/z 96.00 13.65 96 cr 29 39 51 63 74 83 l 115 126 139 152 । 176 | 0- 11 u . j. U , | . U i.., T* 11 p M , rl’i "Ht IIH I’l ■ 1111 in ■ I > I > > 111 > I'l rri I |*l ri [ I1!1! 111 rH | ■ 1 "II’T miz-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance। #125842: Phenanthrene, 2-methyl- 192

22.20 22.40 22.60 22.80 5000 m/z 193.00 12.32

96 , 27 39 51 • 63 82 1 115 126 139 152 165 176 I 0- > p । . । । । ,, u > 11 u u p i, 11 i l’l > il‘s it!, I'l. J... . I . .., I u u ! u . .’I n u ]•! i u I i'n' i | i ill p i u]ir miz-> ;2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance> #80999:5H-Dibenzo[a,d]cycloheptene 192 22.20 22.40 22.60 22.80 m/z 146.10 11.79% 177 5000

89 165 39.51 63 76 J j02 115 128 139 152 „| J. , o1apanlapondqgonnifonnn t’r. ।, rh / dr ii. 11... । h । < । r n, rr, >, rh 111II । rlll । rlljr up, miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22,20 22.40 22.60 22.80

12474.D 052202.M Thu May 30 10:43:01 2002 Page 16

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GCMS analysis results for sample AE12472, June 2002 · Box DEP Box 15

NYC-WTC_000014054

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12472 conducted on June 4, 2002.

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