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GCMS analysis results for sample AE10813, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10813 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000046064–000046080

Folder label: “GCMS X 5/7/02 A 5/15/02

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NYC 9/11 Public Portal Document

- Data File : C:\MSDCHEM\1\DATA\051402\10813.D vial: 23 Acq On : 15 May 2002 8:17 am Operator: Mclean Sample : 5/7 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 6 Phenanthrene, 9-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.30 ug/L 372342 Phenanthranene - dl 0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Anthracene, 9-methyl- 192 C15H12 000779-02-2 50 3 Benzene, 1,1'-(1,2-propadienylid... 192 C15H12 014251-57-1 47 4 2,5-Dihydrophosphole , 3-methyl-1... 192 C11H13OP 1000196-97-5 45 Abundance Scan 3319 (22.580 min): 10813.D (-3312) (-) m/z 192.10 100.00% 192

5000

. 96 146 160 TT ATd ■ 'i ■ 82 । 1 22.20 22.40 22.60 22.80 23.00

m/z-> 0 TI r 1111 42 54 + 66 '11111111*!" r 108 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■111' ‘'11'111 r ' Me —— m/ z 191.10 21.14%' Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 23.00 m/ z 193.00 17.40% 96

mlz-> 0 29 39 51 63 74 83 TImmu—uutm— — — —trtou— l OmtpTTTrT 115 126 139 152 TT—TTETOONTTNTTTgT 165 1 ■ i'1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 + Abundance #125849: Anthracene, 9-methyl- 192

22.20 22.40 22.60 22.80 23.00 5000 m/ z 146.10 14.65%

96 165 । 28 39 51 63 74 83 I 105 115 126 139 152 I 176 I Ol '“I 1 1 il | 1 1 1 '*| ' ITi r ■ ■ '"| lli i । i I’l't ′′ l‘l'] 1l i’| i । I I [ ri't । | i i ri | t i r i']r ri i |'I t i r | iTl i । i rtt । i t tij i i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125850: Benzene, 1,1’-(1,2-propadienylidene)bis- .......... A. 192 22.20 22.40 22.60 22.80 23.00 m/z96.10 13.79% 5000

165 an 94 115 26 39 _ 51 , 103 63 74 83 . 1 126 139 152 -176 0 ■ ............lrlp 111 n I ‘ ‘‘I 'll I I I I l t I TTTpr T1 ‘III /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

10813.D 050102.M Thu May 16 14:15:51 2002 Page 9

NYC-WTC_000046077

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NYC-WTC_000046077Source: NYC Law Department, mirrored locally

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