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GCMS analysis results for sample AE10163, May 2002

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Laboratory report showing GC/MS analysis results for sample AE10163 including surrogate recovery data on May 14, 2002.

NYC-WTC_000023472–000023486

Folder label: “GCMS X 5/9/02 A 5/13/02

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NYC 9/11 Public Portal Document

’ Data File : C:\MSDCHEM\1\DATA\051302\10163.D Vial: 11 Acq On : 13 May 2002 7:38 pm Operator: Mclean Sample : 5/9 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Phenanthrene, 9-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 22.58 0.28 ug/L 333009 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53—-/ 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 45 A 3 Anthracene, 1-methyl- 192 C15H12 000610-48-0 42 / 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 Abundance Scan 3319 (22.580 min): 10163. D (-3313) (-) m/z 192.10 100.00% 192

5000

1 । ■ 82 96 146 160 --H 4 118 22.20 22.40 22.60 22.80 23.00 42 54 70 0 TIWPPPTTTTTHHT •‘ | 1 ■ u I I I I I | I I I I | m/z 191.10 20.51% mfe-> 10 20 30 40 50 60 70 80 90 100110120 130140150 160170 180190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 > I ' ‘ 1 1 I ' 22.20 22.40 22.60 22.80 23.00 m/z 193.10 14.34% 96 ig5 । . 29 39 51 63 74 83 J 115 126 139 152 | 176 B Of TPWTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT111—3 miz-> 10 20 30 40 50 60 70 80 90 100110120 130140150 160170 180190 200 Abundance #80965:2,5-DihydrophosphoIe, 3-methyl-1 -oxo-1 -phenyl- 192 164 1 I ' ' ' ' I ' ' 1 1 1 1 1 1 1 1 1 22.20 22.40 22.60 22.80 23.00 5000 99 m/z 146.10 13.22% 115 47 77 177 67 125,34 146 m/z—> 0 -27384574+ mlrrll mr Ail r—4,1155, TTTT 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180190 200 U Abundance #125854: Anthracene, 1-methyl- -------------------------- 192 22.20 22.40 22.60 22.80 23.00 m/z 96.00 11.25% 5000

82 94 165 18 27 39 51 63 | || 115 126 139 150 I 176 „ 0 TI—u91——0——TTd000—0——0—g—HTTHDTTTHTTTTTTHTTH ‘i 1 1 1 I | I । ■ ' i 1 m/z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160170 180190 200 22.20 22.40 22.60 22.80 23.00

10163.D 050102.M Tue May 14 11:41:25 2002 Page 7

NYC-WTC_000023483

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NYC-WTC_000023483Source: NYC Law Department, mirrored locally

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