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GCMS blank analysis results for May 2002

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank run conducted on May 14, 2002, showing non-detect results for various compounds.

NYC-WTC_000022965–000022989

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000022978
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NYC 9/11 Public Portal Document ~pul A\SDO

Data File C:\MSDCHEM\1\DATA\050902\0508LB.D Vial: 4 Acq On 9 May 2002 5:43 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 7 Phenanthrene, 9-methyl- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 22.58 0.25 ug/L 280257 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 45 2 3-(2-Methoxy-5-methylphenyl)acry. .. 192 C11H1203 103986-76-1 42 3 Anthracene, 1-methyl- 192 C15H12 000610-48-0 42 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 Abundance Scan 3319 (22,580 min): 0508LB.D (-3312) (-) m/z 192.10 100.00% 192

5000

42 70 8.2 96 1 118 146 160 m 22.20 22.40 22.60 22.80 23.00 mTT — 0 ' I" " 11 ■" I ■1111' 11 ‘ ■1 [ >11111111 / 111! 111111111! 1111 j ।1 ‘ m/z 191.10 18.04% m/z-> 10 20 30 40 50 60 70 80 90 100110 120130140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 1912

5000 ............ *,..0 22.20 22.40 22.60 22.80 23.00 m/z 146.10 16.61% 96 165 i । 29 39 51 J 63 74 83 115 126 139 152 | 176 . 0! ■ i" " i" "i1'" i'“1 r1'111'1" 'ii’!i "ll i 11 r ।.' 11 itt । ■ 11 j 1111'| > 111 r> > > • j i1' "i' ri i’r T’I" n/z-> 10 20 30 40 50 60 70 80 90 100110 120130140 150 160 170 180 190 200 Abundance #80954:3-(2-Methoxy-5-methylphenyl)acrylic acid 161 192 ,..... .0. 22.20 22.40 22.60 22.80 23.00 5000 105 m/z 96.00 14.17% 77 132 91 115 , 145 39 51 65

Wz-> 0 ' i" " i" " i ■" I., In, ‘ I' ■■ ■ i 44 । ll, । mrkei — 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 . 175 kd. 1 >■' ■ r11’ i11" r Abundance #125854: Anthracene, 1 -methyl- 1 i 1 ■ ■ ■ i TIE 192 22.20 22.40 22.60 22.80 23.00 m/z 193.10 13.57%

5000

82 94 165 18 27 39 51 63 , I ll 115 126 139 150 I 176 „ - 0 -ICI*"p]mhhm mfe-> 10 20 30 40 50 60 70 80 90 100110 120130140 150 160 170180 190 200 22.20 22.40 22.60 22.80 23.00

0508LB.D 050102.M Tue May 14 10:14:56 2002 Page 10

NYC-WTC_000022978

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NYC-WTC_000022978Source: NYC Law Department, mirrored locally

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