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GCMS analysis results for sample AE09575, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE09575 conducted on May 14, 2002.

NYC-WTC_000023130–000023147

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023140
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NYC 9/11 Public Portal Document

. Data File C:\MSDCHEM\l\DATA\050902\9575.D Vial: 11 Acq On 9 May 2002 11:26 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 3 Phenanthrene, 9-methyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 22.58 0.34 ug/L 538484 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 45 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 4 Anthracene, 9-methyl- Abundance Scan 3319 (22.580 min): 9575.D (-3311) (-) 192 C15H12 192 000779-02-2 40 - m/z 192.10 100.00%l 9 5000

96 146 160 ...... A.... / 22.20 22.40 22.60 22.80 23.00 42 51 70 82 O 'I"........... . ....................... ■ 111li11[. TWPTTITTTTTTTTTTHTT — 122 -H m/Z 191.10 21.70% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

\ 5000 22.20 22.40 22.60 22.80 23.00 m/z 193.10 15.14% 29 39 51 63 74 83 T 115 126 139 152 165 176 | | O+ ' I " " I " " r " ' I " " I ' r ri' r1 ' '11' 11 > I n I | I I ri 11 > I 111 11 I |'| I I I I I'l I I I I i’i'i I I I rl I I i i'l | I! T’i’ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965:2,5-Dihydrophosphole, 3-methy!-1-oxo-1 -phenyl- 164 192 ..... n....n, 22.20 22.40 22.60 22.80 23.00 5000 99 m/z 146.10 14.51%| 115 47 77 177 67 125,3, 146 0 —2738 Ima +7+—l T4441,111341,41,455,, —m ‘1’3 n/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 m 22.20 22.40 22.60 22.80 23.00 161 m/ z 96.10 11.55%

5000

77 91 121 149 177 103 138 52 64 0 mm 11‘A 1 II 4 ,...... |...... , I' 1 " I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

9575.D 050102.M Mon May 13 11:51:00 2002 Page 6

NYC-WTC_000023140

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NYC-WTC_000023140Source: NYC Law Department, mirrored locally

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