GCMS reference analysis results for sample AE09329, May 8 2002

NYC 9/11 Public Portal Document

- Data File C:\MSDCHEM\1\DATA\050202\9329.D Vial: 9 Acq On 2 May 2002 6:08 pm Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Phenanthrene, 9-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.34 ug/L 442392 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- ' 192 C15H12 000883-20-5 45 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 42 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 4 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 42 Abundance Scan 3319 (22.580 min): 9329. D (-3312) (-) m/z 192.10 100.00% 192

5000 ........ . .... A 42 52 70 82 “ i- 96118 1 60 146II 22.20 22.40 22.60 22.80 23.00 I | I I r I | i I i | | | | i i | I I 1 I | T I It | I t I i | I I i I | 1 I I i | i i i I | i i i I | i i i i | f i i i | i i i i | i i i I | i I i i | i i i i | i i i i | m/z 191.10 17.86% /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 1 1 1 ' ' 1 I ‘ 1 "61" 1 1 1 I ' 22.20 22.40 22.60 22.80 23.00 m/ z 193.10 15.74% 96 165 i । 29 39 51 63 74 83 l 115 126 139 152 । 176 I 1 | 1 1 1 1 [ 1 1 1 1 | i r i 1 [T I 1T I’rri [ ITTf* i I' I | 1 II I | 7 I 1 I | 1 11 1 | if 1 1 | 1 | 1 1 | r r i i |l i 1 1 [ i'l 1 1 । i ill । 1 ; (I, 4 11111 /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125842: Phenanthrene, 2-methyl- 192 -

22.20 22.40 22.60 22.80 23.00 5000 m/z 96.10 14.78%

82 96 . 27 39 51 63 - 1 115 126 139 152 155 176 I [ ) I I i | i i I I | I | i । | > i > i | i I I I | i r i i | I i i i | > I I i ‘ i " " i1 " ' i'' " i" " i" I r 1'111 1' 111 mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125849: Anthracene, 9-methyl- 192 22.20 22.40 22.60 22.80 23.00 m/z 146.10 13.70%

5000

_ 96 165 28 39 51 1 1 1 |63 I | 1 1 1 I | I 1 I I'| f I 1 ' 74 83I'l'l 1 IJI l | 105 i'l l I | 1 t’t j'l'l 115 126 139 152 j 176 1 1 | | | | ’i*i r | 1 1 I 1 । । । । । ’। r 1 1 > |ll 1 I j I I I 1 | 1 1 l | | 1 i l l ............... A........... / ’11" 1 । 1 ■ ■ ' । '1 1 ■ । 1 1 ' 1 । 1 1 1 1 । ' /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

9329.D 050102.M Mon May 06 13:54:23 2002 Page 8

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