GCMS reference analysis results for sample AE09329, May 8 2002

NYC 9/11 Public Portal Document

- Data File C:\MSDCHEM\1\DATA\050202\9329.D Vial: 9 Acq On 2 May 2002 6:08 pm Operator: Mclean Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 5 Anthracene-d10- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.58 ug/L 763990 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 93) 2 Phenanthrene-dlO 188 C14D10 001517-22-2 80 Z 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 4 Benzaldehyde, 2,5-difluoro-4-hyd... 188 C8H6F2O3 148872-77-9 47 Abundance Scan 3409 (23.109 min): 9329.D (-3402) (-) m/z 188.15 100.00% 188

5000 ........../............................. । * । । । । । । । । T । । i r t i ] r i i । । 80 94 22.80 23.00 23.20 23.40 43 57 66 — .1 ............. 132 146 ,, 160..... 11 । i । । i । i । । i । i i 'r i■|-ti i i । 7 f i'i । i f I i । i I I I I । I ■i । । I I । । I I > I I I I I I I I I I I I I ( I I I I I I > I I I I I I I > I ' I I I I m/ z 94.05 17.71% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/Z 189.10 14.61% 80 94 160 | 17 30 42 52 ° | 108 118 132 146 I 170179 'i | ri 1 i | ri । । | । i n | t i i । | I I 1 । | । I I t-| r ri I | tTTrfTTmt t rrtpn-t p riT| !•» f i p i t r । i i "l‘‘i i i i | i i i t | I’f’l 11001]

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ........../ 22.80 23.00 23.20 23.40 5000 m/z 80.05 13.09%

80 94 160 30 42 52 66 , . 108 118 132 । i146 I 170179 | ip i r i | i 1 > i | << I I | I | I | | I I > I | I I I I rTf 1111 | I ri । | I i ri । i 11 11 r i i i |' I" n' i i i ITM*"‘!"I । । | । । । । |'ll I I | । j । a n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- .00.0/ 188 22.80 23.00 23.20 23.40 117 m/z 184.05 104 12.95% 91 160 5000 131 170 27 3|9 51 65 78 145 Hr n , 111 I, 11 ll । Alp ml i't r Hll TIT 4 rn /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9329.D 050102.M Mon May 06 13:54:23 2002 Page 9

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