GCMS analysis results for sample AE10815, May 2002

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Gas chromatography-mass spectrometry report for sample AE10815 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000046094–000046111

Folder label: “GCMS X 5/7/02 A 5/15/02”

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NYC 9/11 Public Portal Document

‘Data File : C:\MSDCHEM\1\DATA\051402\10815.D Vial : 25 Acq On : 15 May 2002 9:55 am Operator: Mclean Sample : 5/7 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene-dlO - Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.50 ug/L 734987 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Anthracene-dlO- 188 C14D10 001719-06-8 93 2 Phenanthrene-dlO 188 C14D10 001517-22-2 87 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3409 (23.109 min): 10815.D (-3401) (-) m/z 188.20 100.00% 188

5000

T i |’ / IV ii J i i 1 1 I 1 ' T r I 43 57 66 80 94 22.80 23.00 23.20 23.40 0 I | I , , ! | I I I I | I I I 7 I r H #IFrHl rPterf I I I f 1 17 I I I-1-1 I I 13214 l m/z 189.10 15.52% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

------- 5000 22.80 23.00 23.20 23.40 m/z 184.10 12.98% e 80 94 160 I, 17 30 42 52 00 I 108 118 132 146 , 170179 0 11 । । । r y i 11 i |'i i i i 11 i i i । I'I, i । fl I i । r i 11 | Prri | Uti | rm I'rmj CFrrrtrtgri i i । । i "I’’ i i i | । । i1 | I'l'l I | । r । TI mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/ z 94.05 10.12%

80 94 160 30 42 52 66 , | 108 118 132 146 II 170179.1,1 | 0 11 [ । । । । । । । । । । । । । I | I । । i । I I । । । rl f । । । i II it i 1 | H । । | i । i i । । । । i । । । । i । Ti i || I II|i I ii | i i II t TFrTr m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- ......... /I 1 ' 1 1 1 1 ' I ' 'n 1 1 1 ' ' 1 I ' ' ' ' I 188 22.80 23.00 23.20 23.40 117 104 m/z 80.10 9.40% 91 160 5000 131 170 27 3i9 51 65 78 145

/z-> 0 111 " ' r ।■ , , 11 h, 11 +,l । hp ml i'i n 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 + " i" ........ /............................. । ■ | 1 1 ' ■ 1 ■ ■ 1 1 | i > ' । | -i r ’*TI 22.80 23.00 23.20 23.40

10815.D 050102.M Thu May 16 14:17:36 2002 Page 11

NYC-WTC_000046109

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NYC-WTC_000046109Source: NYC Law Department, mirrored locally

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