GCMS analysis results for sample AE09572, May 2002

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* Data File C:\MSDCHEM\l\DATA\050902\9571.D Vial: 8 Acq On 9 May 2002 8:59 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.47 ug/L 824160 Phenanthranene- dl 0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 2 Phenanthrene-diO 188 188 C14D10 C14D10 001719-06-8 87 ) 001517-22-2 86 4 0 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 Abundance Scan 3409 (23.109 min): 9571.D (-3402) (-) m/z 188.10 100.00% 188

5000

80 94 m.. | 22.80 23.00 23.20 23.40

m/z-> 43 54 66 0 TmTTTTTTTTTH | । 42 m . 207 ' 1“11 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 m/z 94.10 16.62% Abundance #79826: Anthracene-d1 0- 188

- 5000 22.80 23.00 23.20 23.40 m/z 189.15 16.20% 17 30 42 52 ° 8094 108118 132 146 160 ,|| 170 0 111111! 111 111J11 n U 1111111111111 H 11111| 1111 |ttTT| 1111 j t NT7tttr IJ11111 H'l'i 111 [ m 111’l"l

m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79827: Phenanthrene-d10 1tS m 22.80 23.00 23.20 23.40 5000 m/z 184.10 13.74%

80 94 160 30 42 52 66 ll 108118 132 146 1 170 0 ''1............ 1...... . u ■ ■ .. ....... -I |... if * I" " I" " I"1 mz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79739: Cycloheptanone, 4-phenyl- ‘ I’’ T4I’’*’I’*’I US 22.80 23.00 23.20 23.40 117 m/z 80.15 11.14% 104 91 160 5000 131 170 27 39 51 65 78 145 . - . 0 rrit । n 11 11 Jh 11 H4+4H+/y ml n n 1 4 1 -rpm- 'I" " I" " I"' m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 22.80 23.00 23.20 23.40

9571 .D 050102 .M Mon May 13 11:48:17 2002 Page 7

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