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GCMS analysis results for sample AE09577, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE09577 conducted on May 14, 2002.

NYC-WTC_000023179–000023194

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023193
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NYC 9/11 Public Portal Document

-Data File : C:\MSDCHEM\1\DATA\050902\9577.D Vial: 13 Acq On : 10 May 2002 1:04 am Operator: Mclean Sample : 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.43 ug/L 487291 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Anthracene-diO- 188 C14D10 001719-06-8 91 2 Phenanthrene-diO 188 C14D10 001517-22-2 91' 3 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 53 4 Benzene, 1-(1-cyclohexen-l-yl) -4... 188 C13H160 020758-60-5 52 Abundance Scan 3409 (23.109 min): 9577. D (-3403) (-) m/z 188.10 100.00% US

5000

42 54 — 66 132 146 160 80 ।94 22.80 23.00 23.20 23.40

/z-> 0 anpaagapphong 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 189.10 17.22% Abundance #79826: Anthracene-d10- 188

................ ..................................... 5000 22.80 23.00 23.20 23.40 m/z 187.10 15.37% 80 94 160 66 17 30 42 52 | | 108 118 132 0 ' I' " 11' " ' I" " 111111' 111 Mlipall | । ' ' 1 | । । ' ' | । । ' । | ' ' ' ' | ' ' ' । | । ' । ■ 146—4179179 — mlz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 US -

22.80 23.00 23.20 23.40 5000 m/z 94.10 14.87%

80 94 160 30 42 52 66 , 0 TIWWTPWTTTTTTTTTTHTTTTH t rt +1198118.132.146—4179179— m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79722: Cyclohexanone, phenylhydrazone its 22.80 23.00 23.20 23.40 93 m/ z 80.10 12.57%

5000 55 65

u 41 77 106 145 29 120 132 ।II, 159 170 0 TTM+H IH 11‘- ■ ' I • T1I*‘II‘‘I m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9577.D 050102.M Mon May 13 11:52:26 2002 Page 10

NYC-WTC_000023193

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NYC-WTC_000023193Source: NYC Law Department, mirrored locally

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