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GCMS analysis results for sample AE10160, May 2002

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Laboratory report showing GC/MS analysis results for sample AE10160 including surrogate recovery data on May 14, 2002.

NYC-WTC_000023454–000023471

Folder label: “GCMS X 5/9/02 A 5/13/02

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NYC 9/11 Public Portal Document

- Data File : C:\MSDCHEM\1\DATA\051302\10160.D Vial: 10 Acq On : 13 May 2002 6:49 pm Operator: Melean Sample : 5/9 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.42 ug/L 477470 Phenant hranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 93 2 Phenanthrene-diO 188 C14D10 001517-22-2 87 3 4H-Pyrido[1,2-a]pyrimidin-4-one,. 188 C11H12N2O 057773-19-0 50 4 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 40 Abundance Scan 3409 (23.109 min): 10160.D (-3402) (-) m/z 188.10 100.00% 188

5000

40 52 66 j4 -|32 158 _ 22.80 23.00 23.20 23.40 0-—mmPTTTTHTTTTTTTTTTHTTTTTTTTHTTT m/z 184.10 16.71% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance> #79826: Anthracene-d10- 188 ...............

5000 22.80 23.00 23.20 23.40 m/z 189.10 16.13% rr 80 94 160 । 17 30 42 52 ° . 108118 132 146 | 170179 i 0 TWWTWITTTmTTTTHTITTmtuott Tuur m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 - 22.80 23.00 23.20 23.40 5000 m/z 80.05 15.85%

80 94 160 30 42 52 66 „ 11 108118 132 146 II 170179,1 0-TTPTHTT —TmTTTT m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79770:4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- ...................................... ............... 145 188 22.80 23.00 23.20 23.40 173 m/ Z 94.10 12.57%

5000 92

65 39 159

m/z—> I 55 i 78 | 0 TIPTH .......... . ■1 ■ r ' " i" " i " ‘ ■ i'1" i HH 119 132 U 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10160.D 050102.M Tue May 14 11:40:53 2002 Page 11

NYC-WTC_000023469

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NYC-WTC_000023469Source: NYC Law Department, mirrored locally

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