GCMS analysis results for sample AE08960, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08960 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049571–000049583

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\1\DATA\020424\08960.D Vial: 11 Acq On : 24 Apr 2002 7:42 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.44 ug/1 845046 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene d10- 188 C14D10 001719-06-8 83 2 Phenanthrene-diO 188 C14D10 001517-22-2 47 3 1,4-Naphthoquinone, 2,3-dihydro-... 188 C12H1202 1000157-22-3 40 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 Abundance Scan 4915 (31.958 min): 08960.D (-4903) (-) m/z 188.15 100.00% 188

5000 40 94 >6680 31,60 31.80 32.00 32.20 1 IPWp132—Pme ‘rp-rrrp-rrrp-rTt 160 Ttttt m/z 40.10 40.43% niz-> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 Abundance #79826: Anthracene-d10- 118

5000 31.60 31.80 32.00 32.20 “ ‘ ‘ m/z 94.20 22.50% 17,..3p...42..52..,.66,.442..1,108,118,122,146,12170179/l Tunr miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188 *BI -------- 31.60 31.80 32.00 32.20 5000- m/z 184.10 15.88%

80 94 160 30 42 52 66 , .108118 132 146 .I., 170179.1,1 mmPmppHHt llI! ■ 111111111111 > 111 |i 1111 n u 11 r’l’t > 11 p 111 "‘‘l Truus mz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79805:1,4-Naphthoquinone, 2,3-dihydro-5,8-dimethyl- 118 TSI mm 31.60 31.80 32.00 32.20 173 m/z 189.20 13.92% 5000 145 82 91 159 27 39 51 65 । 105 15 131 iz—> ......... I...... I. I ■ rteln, , r# ., i-lUl 11 mr । ■ nl ।. mb 11 ■ ll ■ ■ । fl I'11 ‘ 11............................................................................................. 11111 ■ ■ "l’t’t 10 20 30 40 50 60 70 80 90 100110120130 140 150 160 170 180 190 ‘Ttttt ‘II ) Ti *■ * * । i * * । 11 31.60 31.80 32.00 32.20

08960.D SCAN020424.M Thu May 02 14:44:29 2002 Page 8

NYC-WTC_000049582

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GCMS analysis results for sample AE08964, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049622

Laboratory report documenting GCMS analysis of sample AE08964 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998