GCMS analysis results for sample AE08962, May 7, 2002

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Data File : C:\MSDCHEM\1\DATA\020424\08962.D Vial: 13 Acq On : 24 Apr 2002 9:39 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.36 ug/1 626302 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 93 2 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 50 3 Phenanthrene-diO 188 C14D10 001517-22-2 49 4 Benzene, 1-(1-cyclohexen-l-yl)-4. . . 188 C13H160 020758-60-5 42 Abundance Scan 4915 (31.958 min): 08962.D (-4908) (-) m/z 188.15 100.00% 188

5000

94 TI p-r-rT-p-r-r-p-rT-r-r-p 40 31.60 31.80 32.00 32.20 66 .1 1 415 “'i"“ TOT ......... . t.... ।......... ।.... ।.... |..!...., । .1 m/z 94.10 19.07% miz—> 20 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #79826: Anthracene-d10- 188 ' --- 5000 31.60 31.80 32.00 32.20

66 94 160 M/Z—40:19.w15:22% 17 42 > ••l* ip' 4413244. ..।.... r ... ।....,.... ।.... ।.... pl.. p ... ।.... p . 111 ll 20 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #79821: Selenide, ethyl 1 -methyl-1 -penten-3-ynyl 108 ‘IB T T T IT 31.60 31.80 32.00 32.20 5000 m/z 184.20 15.07% 79 159 +4444.4/97314.4. miz-> 20 40 60 80 100 120 140 160 180 200220240 260 280 300320 340 360380 400420 Abundance #79827: Phenanthrene-d10 ‘I T PT) T-p-r-r-r-p-r-r-T-j-r 108 31.60 31.80 32.00 32.20 m/z 80.05 12.51% 5000

801 160 | 100 132 1 jj miz—> 1130,52/14 **mpmmm,gppmin 20 40 60 80 100 120 140 160 180 200220240260 280 300320 340360380 400 420 1iI 11II 31.60 31.80 32.00 32.20

08962.D SCAN020424.M Thu May 02 14:47:58 2002 Page 8

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