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GCMS analysis results for sample AE08964, May 7, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08964 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049622–000049633

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020424\08964.D Vial: 15 Acq On : 24 Apr 2002 11:37 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.35 ug/1 623020 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthra ne-dlO- 001719-06-8 91 188 C14D10 2 Pentac yclo[7.3.1.1. (4,12) .0 (2,7) . . . 188 C14H20 1000215-61-8 52 3 Selende, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 50 4 Antipyrine 188 C11H12N2O 000060-80-0 50 Abundance Scan 4915 (31.958 min): 08964.D (-4903) (-) m/z 188.10 100.00% 188

40 50)0

80 94 TF i ■ • ■ 1 i • ‘ ■ i ■ ■ 1 ■ i “ 158 mlm l 51 66 I I 3160 31.80 32.00 32.20 108 132 HttmTTm —nguT m/z 40.10 Wy~WMAMWWMe 54.77% m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 1(8

5000 1dnn//——mmnnnI/m 31.60 31.80 32.00 32.20 m/z 184.10 16.94% RR 80 94 160 | 17 30 42 52 P J , 108118 132 146 I. 170179 , J TI—Pmmm]—uag—mngut—m—atgm—nmanpT“gttn trrrq iz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79715: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... 1(8 ’ii I ■ ■ |-r 1*4*44*1* 31.60 31.80 32.00 32,20 5000 79 91 m/z 94.00 16.79% 55 67 105 131 I 117 145 159- mm# --HHH133.— mfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79821: Selenide, ethyl 1-methyl-1-penten-3-ynyl 1(8 P 31.60 31.80 32.00 32.20 m/z 189.20 14.84%

5000 79 91 107 119 145 159 173 11* TOTNOt 131--4--4ml+# Trrq - ■111 • •1 ■ । • • ■ ■ । • n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140150 160 170 180190 31.60 31.80 32.00 32.20

08964.D SCAN020424.M Thu May 02 14:53:05 2002 Page 7

NYC-WTC_000049632

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NYC-WTC_000049632Source: NYC Law Department, mirrored locally

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