GCMS analysis results for sample AE08959, May 7, 2002

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'Data File : C:\MSDCHEM\1\DATA\020424\08959.D Vial: 10 Acq On : 24 Apr 2002 6:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.28 ug/1 554943 Phenanthrene-dl0 31.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 83 2 Antipyrine 188 C11H12N2O 000060-80-0 38 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 33 4 Phenanthrene-diO 188 C14D10 001517-22-2 27 Abundance Scan 4915 (31.958 min): 08959.D (-4908) (-) m/z 188.20 100.00% 1(6

5000

94

niz-> p.,52.s,4 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 T-rrj-rrrrpT 132 TphrT7 158 T1‘ l ‘ ‘‘ 3160 31.80 32.00 32.20 m/z 94.10 21.27% Abundance #79826: Anthracene-d10- 188

5000 TI TOunmnnT 3160 31.80 32.00 32.20 m/z 189.20 17.53% — 80 94 160 । 17 30 42 52 P . J 108118 132 146 ,1. 170179.1, । h I I 111 | 1111 [ Il II | I I I I | I 1 I I | I I I I | 1 1 Ittrrt[i I I I | I Ul | ■ I I I | I I I I |I I I I | I I FTrt’t I I I ] 11 ■ ■ |I1I'I‘ trrrr

iz—> 10 2030405060708090 100110120130140150160170180190 Abundance #79725: Antipyrine 1(6 96 —I ------- 31.60 31.80 32.00 32.20 5000 m/z 92.00 11.99% 77 56 105 39 27 09 67 . , Ji 115 130 145 159 173 j TITpntp -H ppmtmtmmmmpm miz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 1(6 31.60 31.80 32.00 32.20 m/z 40.10 10.185 5000

115 143 rTTTTTTTTTrITT^p^TTTp4HnTr^^ 158 170 Vttt tt+tt n/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 31.60 31.80 32.00 32.20

08959.D SCAN020424.M Thu May 02 14:41:19 2002 Page 7

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