GCMS analysis results for sample AE08959, May 7, 2002

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•Data File : C:\MSDCHEM\1\DATA\020424\08959.D Vial: 10 Acq On : 24 Apr 2002 6:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 4 Phenanthrene, 9-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.32 ug/1 629292 Phenanthrene-diO • 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 72 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 64 3 1H-Indene, 2-phenyl- 192 C15H12 004505-48-0 59 4 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 Abundance Scan 4767 (31.088 min): 08959.D (-4759) (-) m/z 192.10 100.00% 192

5000 40 ................................. .......... 96 146 . 30.80 31.00 31.20 31.40 49 70 82 118 | 160 1111" I"1 tpmmmpmdmtpmmmm Hpr m/z 40.10 36.16% miz-> 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 1512

5000 30.80 31.00 31.20 31.40 m/z 191.10 28.38% 29 39 51 63 74 83 . 7 115 126 139 152 165 176 J | j > 111"| j i j j*| 11 j i i'j 11 y 111»111 i*i i pi i >*l*| rl 1 1jadasj rri 111111 j i t r t‘j r 11 j |‘! 11 > । r’I’ 111 rlt 111111 111 j j i miz-> :20 30 40 50 60 70 80 90 100110120 130140150160 170 180 190 200 Abundance• #125842: Phenanthrene, 2-methyl- 192 1 30.80 31.00 31.20 31.40 ' 5000 m/z 96.15 18.70%

96 ,

miz-> 27 39 51 63 82 ,1 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 115 126 139 152 19 176 । U Abundance #125852:1 H-Indene, 2-phenyl- 192 30.80 31.00 31.20 31.40 m/z 146.20 16.10% 5000

27 39 51 63 74 83 96 115 126 139 152 155 176 1191111—9—1——1m0—800*m30009Hmm “TCTEmmpmmf TTIyur /z—> 20 30 40 50 60 70 80 90 100110 120 130 140150160 170180190 200 30.80 31.00 31.20 3140

08959. D SCAN020424.M Thu May 02 14:41:17 2002 Page 6

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