GCMS analysis results for sample AE09156, May 2002

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■ Data File : C:\MSDCHEM\1\DATA\020424\09153.D Vial: 22 Acq On : 25 Apr 2002 6:29 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 7 Phenanthrene-diO Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.31 ug/1 612074 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 72 2 Anthracene-dlO- 188 C14D10 001719-06-8 72 3 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 40 4 Pentacyclo[7.3.1.1. (4,12) .0(2,7) ... 188 C14H20 1000215-61-8 39 Abundance Scan 4914 (31.952 min): 09153.D (-4905) (-) m/z 188.15 100.00% 188

5000

80 94 T"T । ■ ■ ■ 1 । ■ ■ > ' । > 1 । ■ 31.60 31.80 32.00 32.20 ... ............. . . 313 11 Tr ■ i ■ 11 ■ i1 1 111 '1 '' i'1 1 11' 11 ' i ■' ■'1 i m/z 189.20 22.60% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79827: Phenanthrene-d10 188

5000 TT 31.60 31.80 32.00 32.20

80 94 160 | m/z .93.95 17.79%

n/z-7 30 52 66 '................. i'. 111. ■ 20 40 60 4108,132464 M ‘I‘‘ ‘4‘1‘‘+‘‘‘‘I7‘ '^r1 >11 t 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79826: Anthracene-d10- 188 TTT ............................................. ■

31.60 31.80 32.00 32.20 5000 m/z 80.10 16.38%

80 94 160 I, .. .................... ..... ... ... /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79821: Selenide, ethyl 1 -methyl-1 -penten-3-ynyl 188 31.60 31.80 32.00 32.20 m/Z 184.10 15.22% 5000

79 145159173 ] I i , TT107 131 "n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.60 31 80 32.00 32.20

09153.D SCAN020424.M Fri May 03 11:00:33 2002 Page 9

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