GCMS analysis results for sample AEO8O6S, May 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020424\08958.D Vial: 9 Acq On : 24 Apr 2002 5:44 pm Operator: Nefliu Sample : sample Inst : Instrumen Misc Multipir: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Phenanthrene-d10 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 31.95 0.43 ug/l 848238 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-d10 188 C14D10 001517-22-2 42 2 Selenide, ethyl 1-methyl-l-pente... 188 C8H12Se 025128-48-7 38 3 Anthracene-dl0- 188 C14D10 001719-06-8 12 4 Benzene. 1-(1-cvclohexen-l-vl)-4... 188 C13H160 020758-60-5 9 bundance Scan 4914 (31.952 min): 08958.0 (-4901) (-) m z 188.10 100.00 18

5000 40 94

66 80 158 31.60 31.80 3200 32.20 m/z 94.05 29.08 nlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130140 150 160 170 180 190 thundance #79827: Phenanthrene-d10 1

5000 31.60 31.80 32.00 32.20 m/z 40.10 27.83% 8094 160 30 42 52 108118 132 146 1 17017 -> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 ¼bundance #79821: Selenide, ethyl 1-methyl-1-penten-3-ynyl 1

31.60 31.80 32.00 32.20 5000 m z 189.20 20.91 7s 159 145 173 91 107 119 131 i/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 bundance #79826: Anthracene-d10- 1 31.60 31.80 3200 32.20 m z 184.10 20.89

5000

80 94 160 17 30 42 52 66 108118 132 146 170179 nlz-> 10 20 30 40 50 60 70 80 90 100110120130140150160 170180190 31.60 31.80 32.00 32.20

08958.D SCAN020424.M Thu May 02 14:39:19 2002 Page 7

NYC-WTC 000049557