GCMS scan report for Method 508, April 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020419\08430.D Vial: 17 Acq On : 19 Apr 2002 11:53 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library- : C:\DATABASE\nist98.1 ******* *.* ************************************************************ Peak Number 5 Phenanthrene, 9-methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.35 ug/1 750139 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 64 2 Anthracene, 9-methyl- 192 C15H12 000779-02-2 59 3 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 45 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 45 Abundance Scan 4767 (31.088 min): 08430.D (-4758) (-) m/z 192.10 100.00% 192

5000

96 1 ■ i 1 ■ 30.80 31.00 31.20 31.40

m/z-> 40 49 0 mpmmmmpt 70 82 ..120... ............ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 96.10 16.81% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 A TTB 30.80 31.00 31.20 31.40 m/z 191.00 16.48% 96 IEE i . 29 39 51 63 74 83 l 115 126 139 152 j 176 I 0- 11 ■ " ' i ■1" r " 11 " ■11" ITTTH TTITT miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125848: Anthracene, 9-methyl- 19/2 -• i ■ • 30.80 31.00 31.20 31.40 5000 m/z 193.10 14.06%

96

z-> 27 39 51 63 82 J 115 126 139 152 j 176 „ 0 TIWTTTICWTTWTTTTTTTTTTgmtt 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 Abundance #125856: Phenanthrene, 1-methyl- 1912 30.80 31.00 31.20 31.40 m/z 146.10 10.39% 5000

96 EE 178 •n/z—> 27 39 51 63 82 1 115 126 139 152 100 0 11'' " I " " I'' " I " " I" I'11'-11TTTTTTTTTTTTTTTTTTH 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U 30.80 31.00 31.20 31.40

08430.D SCAN020418.M Mon Apr 29 08:29:49 2002 Page 20

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