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GCMS Method 508 scan results, April 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS scan data for deuterated surrogate compounds in sample AE08487 analyzed on April 19-26, 2002.

NYC-WTC_000023304–000023315

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023312
OCR text

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020419\08487.D Vial: 24 Acq On : 20 Apr 2002 6:46 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 8 Phenanthrene, 9-methyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 31.08 0.32 ug/1 625406 Phenanthrene-dl0 31.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 45 3 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 45 4 Anthracene, 9-methyl-____________________ 192 C15H12 000779-02-2 45 Abundance Scan 4766 (31.082 min): 08487.D (-4758) (-) m/z 192.10 100.00% 19 2

5000 40

96 146 ... a... iz-> 0 ITTmTTmN .... s6,“?.al. 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 118 132 160 pmtptm 0011 l.,. 30.80 31.00 31.20 31.40 m/ z 40.10 37.27% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 30.80 31.00 31.20 31.40 m/z 193.05 16.55% 96 165 । , .......... 29 39 51 63 73 ............ 126 139 152.,, . 176 .., 0 TTpTTnpTTTpTTTpTTrpTTTpTTTpriTp-trqTrrtYrrrrpTTTpT-rTp^ TTjrr mlz-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #125844: Anthracene, 2-methyl- 192

30.80 31,00 31.20 31.40 5000 m/z 146.10 15.68%

m 96 165 Y l 115 139 150 J 176 _ 0 " i" ■ ■ i'1 ■ ■ i" " i' ■'11" " i" " i63" i1 r''1 l'l1 i‘r 1111111 .. . ......... n 11 11 u !‘| n 11111 11! i1!1! > 111 11111 i'I1 TI‘8 n/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80862:1,2-Phenylene diisothiocyanate 1912 30.80 31.00 31,20 31.40 m/z 96.0.0 14.23% 64 5000

39 50 134

/z-> 0 -4.18.44444+r 122 mhpulj 148 160 .,... 11.... | । । ।■>>■। 0 10 20 30 40 50 60 70 80 90 100110120130140150160 170180190200 30.80 31,00 31.20 31.40

08487.D SCAN020418.M Mon Apr 29 08:36:52 2002 Page 26

NYC-WTC_000023312

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NYC-WTC_000023312Source: NYC Law Department, mirrored locally

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