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GCMS analysis results for sample AE10704, May 20 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report for sample AE10704 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000045793–000045810

Folder label: “GCMS X 5/3/02 A 5/13/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020513\10704.D Vial: 15 Acq On : 14 May 2002 2:23 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Anthracene, 2-methyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.35 ug/1 46709 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 58 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 53 3 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 50 4 Bitoscanate 192 C8H4N2S2 004044-65-9 50 Abundance Scan 4767 (31.088 min): 10704.D (-4757) (-) m/z 192.05 100.00% 192

5000

84 146 T*TTT It-I ..... . ............................... . 325 30.80 31.00 31.20 31.40 1I1T TTTTTTTTTTTTTTTTTTTWTTIWWTTITT m/z 191.10 18.55% n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #81034: Anthracene, 2-methyl- 192

5000 ■ ■ i ■ ■ ■ ■ i ■

30.80 31.00 31.20 31.40 82 165 m/z 146.10 18.04% 18 39 . 63 . L 98 115 139. . J. . J PT ■111 "' ।1 ■ "I T 1Th । MAti । r 111 rli +11 n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #125847: Anthracene, 2-methyl- 192 1 ' i ' ' ■ ■ i ■ ■

30.80 31.00 31.20 31.40 5000 m/z 160.10 15.30%

2 . 96 ._ 1 65 I 28 44 6381, 115 139 । ' 1111 ' ' I ' 11 1 | 1 1 1 1 | 1 ' 1 " | 1 Ir1 | 171 1 1 ] I l l'll rl 1 'I ] l l ' n/z->______ 20 Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 #81040: Phenanthrene, 1-methyl- 192 I...... 1 I I I I ' [ > < ' i ' ■ 1 ' i ' ■ 30.80 31.00 31.20 31.40 m/z 193.00 12.70%

5000

95 165

m/z-> TTpr 39 I I | r I I । | । I > t | iT i I |

20 40 60 80 . I, 63 ll I ». j II ll., || II,. 115 . I i < I | I 139 I I I_____ III i | I I I

100 120 140 160 180 200 220 240 260 280 300 320 TH I " 11111'11 LA 30.80 31.00 31.20 31.40 .......... 1 ' I ‘ ' 1 1 1 1 1

10704.D SCAN020507 .M Wed May 15 09:01:18 2002 Page 6

NYC-WTC_000045802

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NYC-WTC_000045802Source: NYC Law Department, mirrored locally

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