GCMS analysis results for sample AE09153, May 2002

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Laboratory report documenting GCMS analysis of sample AE09153 conducted on May 8, 2002.

NYC-WTC_000046405–000046419

Folder label: “GCMS X 4/17/02 A 4/24 - 4/26/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\020424\09152.D Vial: 21 Acq On : 25 Apr 2002 5:30 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene, 2-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.10 0.32 ug/1 606345 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 59 3 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 59 4 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 50 Abundance Scan 4768 (31.094 min): 09152.D (-4759) (-) m/z 192.10 100.00% 192

5000 40 T-r-j-r-r 82 96 146 160 30.80 31.00 31.20 31.40 54 66 I I ll ' i " 11 r 111 I I l > | > f > I | > I > | > < 1 1 | H ’ 1 | 1 I I'1 | 1 1 > > ] I ' FITTT ! | I i n । , IT, | । b .... | — m/ z 40.10 36.98% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125847: Anthracene, 2-methyl- 192

5000 ■ 1 i 1 ' 30.80 31.00 31.20 31.40 m/z 191.10 23.33% 4 CE 28 39 51 63 82 96 115 126 139 152 । 176 TITTHTTTTTTTTTTTTTTTTTTTTT TVTTTIUTPTTWTTTTTTTTTTTTTT TTT /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 192 164 ‘TI > ■ i ■ ■ 30.80 31.00 31.20 31.40 5000 99 m/ z 82.00 13.74% 115 47 77 177 67 146 / — 2739 57. 187, lrl Alpr125,134 155, I— + U 44 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81030: 4-Hydroxy-3,5-dimethy!cinnamic acid TH 1IIIII 192 30.80 31.00 31.20 31.40 m/Z 160.10 13.18%

5000

89 175 ar 63 117 145 45 | 77 105 135 ■I | n'n | rhp ri i | "" 11 I |L 163 I I I | !'| I 1111111" " i TIT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

09152.D SCAN020424.M Fri May 03 10:59:29 2002 Page 7

NYC-WTC_000046415

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