GCMS analysis results for sample AE09153, May 2002

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Laboratory report documenting GCMS analysis of sample AE09153 conducted on May 8, 2002.

NYC-WTC_000046405–000046419

Folder label: “GCMS X 4/17/02 A 4/24 - 4/26/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020424\09152.D Vial: 21 Acq On : 25 Apr 2002 5:30 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.45 ug/1 849649 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthreene-d10— 188 C14 D10 001719-06-8 87 2 Phenanthrene-diO 188 C14D10 001517-22-2 86 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 Abundance Scan 4915 (31.958 min): 09152.D (-4905) (-) m/z 188.15 100.00% 188

5000

80 94 Ti I ' 1 ’ll C"I I I I I I I I I 31.60 31.80 32.00 32.20 40 51 -HH 108 158 66 111"11" " i"1 'r "1 i‘H" i ■ ■ ■ /1" ■' i ■ ■ ■ ■ i••■■ i ■ ■ ■ ■ i ■ ■ 11 /.। . m/ z 94.20 19.30% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 TT I‘‘ITI-II‘IIIIII 31.60 31.80 32.00 32.20 m/ z .80.10 13.93% 66 80 94 160 , |.

n/z-> 17 30 42 52 IT 11111111111 >1111111111 mtH | | 108 118 132 tTT|-f|lll I | I nip 11-1! II I I |l I I

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 146—4179179 — Abundance #79827: Phenanthrene-d10 188 TT I ’ ' I ' 1 1 1 1 1 1 1 1 1 1 31.60 31.80 32.00 32.20 5000 m/z 189.20 12.51%

80 94 160 | 30 42 52 66 il 108 118 132 TTTT146..................... ‘ i' " ' r " ' r | । | | I | | | | 11 i i | | I I i | n-l-l [ I i i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime TT । 1 • |_| । ' 1 1 1 । 1 1 1 1 । 1 188 31.60 31.80 32.00 32.20 m/ Z 184.10 11:03%

5000 143 51 . 64 76 89 | 102 115 J|, 130 ' I " ' ' I " " t " " I " " i1' " 11 d' ' rr 11'1111 > > > > | < 11 > I > ( ' r Hl]1 1111'111 >■" > 111 11" ) "ii 158 170 T I ' ' "H i I I I I I I I [ I m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32 20

09152.D SCAN020424 .M Fri May 03 10:59:31 2002 Page 8

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