GCMS analysis results for sample AE10024, May 2002

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Laboratory report documenting GCMS analysis of sample AE10024 conducted on May 14, 2002, identifying unknown compounds.

NYC-WTC_000044179–000044190

Folder label: “GCMS X 4/26/02 A 5/8/02”

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NYC 9/11 Public Portal Document

' Data File C:\MSDCHEM\1\DATA\020507\10024.D Vial: 23 Acq On 8 May 2002 9:48 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.33 ug/1 36711 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 74 2 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 47 Phenanthrene-diO 188 C14D10 001517-22-2 43 4 -G4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 40 Abundance Scan 4914 (31.952 min): 10024.D (-4907) (-) m/z 188.20 100.00% 188

5000

mlz-> 40 52 64 . ..................... I'' । l"''!. . ........ .. 78 160 11" " i " " I" " I " " I " I1’I'" " 111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TT „l 31.60 31.80 32.00 32.20 m/ Z 94.20 19.86% Abundance #79826: Anthracene-d10- 188

5000 31.60 3180 32.00 32.20 m/z 189.10 14.69% 80 94 160 | 17 30 42 52 00 1 ( 108 118 132 146 I. 170179, । | । i । । | i ii । | । । । I | I i । I | I I r r ] I ttrprtl 11 J i I J Mi | I i I I | i i 11 | > I i i । I I I i । i । I i । FTT""T I i i | i i r i [ |‘l t TIIi m/z-> 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188

145 31.60 31.80 32.00 32.20 5000 m/z 184.10 13.40%

117 41 51 63 77 89 102 130 159 173 Il... ----------------------- "I" " i /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 4 31.60 31.80 32.00 32.20 m/z 92.00 10.60% 5000

80 94 160 30 42 52 66 . . 11 . 108118 132 146 I 170179,1,1 | TTh i । । । । t r । | । i । > | I i > i | I I I I |'l I ri | I I H I i ■ "I 111 । । | I । I । । । । i r | । | । । | I i । i | | । t'l । i iTl'p'i । i | i i । i |,l1l I 11 i । i ’T TTT 1——— /z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10024 .D SCAN020507.M Tue May 14 08:46:00 2002 Page 7

NYC-WTC_000044189

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NYC-WTC_000044144

Laboratory report documenting GCMS analysis of sample AE10021 conducted on May 14, 2002, identifying unknown compounds.

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