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GCMS analysis results for sample AE10066, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE10066 conducted on May 14, 2002, including surrogate recovery data.

NYC-WTC_000044215–000044226

Folder label: “GCMS X 4/26/02 A 5/8/02

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Scanned page image, NYC-WTC_000044225
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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\020507\10066.D Vial: 26 Acq On 8 May 2002 12:45 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.33 ug/1 33118 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 80 2 Pentacyclo[7.3.1.1. (4,12) .0(2,7) . . . 188 C14H20 1000215-61-8 42 3 Phenanthrene-dlO 188 C14D10 001517-22-2 39 4 1-Naphthalenecarboxylic acid, 7- . . . 188 C11H8O3 002623-37-2 35 Abundance ' Scan 4916 (31.963 min): 10066.D (-4908) (-) m/z 188.15 100.00% 188

5000 80 94 TT I ' ' ' 1 I ' ' ' ' I r ' 1 1 I 1 40 55 66 119 131 146 160 170 31.60 31.80 32.00 32.20 ‘i"111 11 " 11 -HHH4 J1111 /1 > ।! । / । > 1111111 > > I'1111111111111 I T’T m/z 80.20 27.82% /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 । | < i । >-[-> i-i-r । "I । । । i । । । । । 31.60 31.80 32.00 32.20 m/z 94.10 23.57% RR 80 94 160 |, 17 30 42 52 P I 1 108 118 132 146 I. 170179. TT । । I | I I I I | I I I I | I I I I | I I I I | I I I I | I I I I | I I I I |‘I i 1 I TTTTI I I I I | 1 | t i j | | | rfry | I i Ppi I I 1 | | I I I | I'rl I | Illi n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1 .1 .(4,12).0(2,7).0(6,11 )]tetradeca... 188 J, l.............. 31.60 31.80 32.00 32.20 5000 79 91 m/z 189.10 23.25% 55 67 105 131 10 117 159

n/z-> ■। JU 1 "11'"11" " r — 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ... ..................................... । 145 173...... ||...... ' i"11 r ' ■11 ’ ’’

Abundance #79827: Phenanthrene-d10 188 31.60 31.80 32.00 32.20 m/ z 92.00 20.47% 5000

80 94 160 30 42 52 66 . 11 108 118 132 146 II 170179,1,1 | 111" I" " I" 111'1" 111" 1111111 i+i 111 I | I I " | H , I | । , U, | I I I ! | I I I ! | ! rl’l"’ I I I | ! I I I | l'l‘llll| 1111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10066.D SCAN020507 .M Tue May 14 08:47:06 2002 Page 6

NYC-WTC_000044225

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