GCMS chain of custody form, sample AE10211, May 2002

NYC 9/11 Public Portal Document

‘Data File C:\MSDCHEM\l\DATA\020509\10211.D Vial: 13 Acq On 9 May 2002 10:29 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.34 ug/1 40849 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10 - 188 C14D10 001719-06-8 72 <2 Phenanthrene-diO 188 C14D10 001517-22-2 59 3 1,4-Naphthalenedione, 2-hydroxy-.. . 188 C11H8O3 000483-55-6 46 4 Benzene, 1-(1-cyclohexen-l-yl) -4... 188 C13H160 020758-60-5 38 Abundance Scan 4915 (31.958 min): 10211 .D (-4905) (-) m/z 188.10 100.00% 188

5000

80 94 36 51 66 no 160 31.60 31.80 32.00 32.20

n/z-> - 1344444 ! 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 312 m/z 94.30 23.79%! Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/z 80.10 21.14%| . 80 94 160

m/z-> 30 ' 1 ' i ' '' ■ T' 20 40 52,96.44 60 118132146 1 'T' ' I " "l " " "‘1‘‘1‘1‘111111111111TT—ETT‘IrIT 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79827: Phenanthrene-d10 188 TI । i । • i । • I > i' ■ ■ j 1 31.60 31.80 32.00 32.20 5000 m/z 189.20 20.34%

80 94 160

m/z-> 52,66. 30 —108. T| 132146 11 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ‘ 11111111170171‘1‘00111—-I0‘ITTT

Abundance #125707:1,4-Naphthalenedione, 2-hydroxy-3-methyl- 188 31.60 31.80 32.00 32.20 m/z 186.10 11.56%

5000

-............................................................ TTT ■ 1 > > P’ ' ' । 1 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.60 31.80 32.00 32.20

10211.D SCAN020507 .M Tue May 14 14:23:36 2002 Page 4

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