Gas chromatography-mass spectrometry report for sample AE10704 showing detection of unknown compounds and surrogate recovery.
NYC-WTC_000045793–000045810Folder label: “GCMS X 5/3/02 A 5/13/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\l\DATA\020513\10704.D Vial: 15 Acq On : 14 May 2002 2:23 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1
Peak Number 5 Anthracene-dlO- Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.36 ug/1 48682 Phenanthrene-dl0 31.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Anthracene-diO - 188 C14D10 001719-06-8 72 2 Ni kel, di-.mu.-carbonylbis(.eta... 302 C12H10Ni2O2 012170-92-2 43 3 Phenanthrene-diO 188 C14D10 001517-22-2 39 4 Cy loheptanone, 4-phenyl - 188 C13H160 067688-28-2 37 Abundanc । Scan 4915 (31.958 min): 10704.D (-4906) (-) m/z 188.20 100.00% 188
5000
94 ' i T 1 ' r 1 1 1 1 'r I 1 1 1 1 11il 1 1 1 1 66 160 31.60 31.80 32.00 32.20 42 ,| ,J ,i 112132 hl i, 299 376 TTTTTTTTTTTTTTTTTTTmt 11" " i1" ' r11' i " " i " " i " '1111111'1111' m/z 94.10 18.99% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79826: Anthracene-d10- 188
5000 > I t ■ 1 r- । ■ ■ > • | > 1 ■ । I > 1 1 > । ' 31.60 31.80 32.00 32.20 m/ z 189.20 18.20% KA 94 160 17—42.,1411141324 ' i" " I " " r " ' i i ■r" ।1"11"11 r11 "IT " i' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79885: Nickel, di-.mu.-carbonylbis(.eta.5-2,4-cyclopentad... 188 M , I 1 I I
246 31.60 31.80 32.00 32.20 5000 123 m/z 66.10 12.39%
58 28 97 1 - 302
m/z-> 77 | TITt 141 - 160 _ _ ":218 'T" " I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 +27444 ■ i• ■ ■■ j■ • " i>
Abundance #79827: Phenanthrene-d10 188 31.60 31.80 32.00 32.20 m/z 80.20 11.88% 5000
80 160 30 52 . 100 132 "1'““' I'" 1''I1'" T rtrt"ut rr IT t l | I'! TTTT4 '11'''' i'1' ‘ r " ' i "111'11111" ' i111111111111" I' /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 | 31.60 31.80 32.00 32.20
10704.D SCAN020507.M Wed May 15 09:01:19 2002 Page 7
NYC-WTC_000045803
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NYC-WTC_000045761
Gas chromatography-mass spectrometry report for sample AE10702 showing detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045707
Laboratory report detailing GC/MS analysis of sample AE10698 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045721
Laboratory report detailing GC/MS analysis of sample AE10699 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045811
Gas chromatography-mass spectrometry report for sample AE10705 showing detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044119
Laboratory report documenting GCMS analysis of sample AE10019 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044227
Laboratory report documenting GCMS analysis of sample AE10067 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044144
Laboratory report documenting GCMS analysis of sample AE10021 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045735
Laboratory report detailing GC/MS analysis of sample AE10700 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044203
Laboratory report documenting GCMS analysis of sample AE10061 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046405
Laboratory report documenting GCMS analysis of sample AE09153 conducted on May 8, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046420
Laboratory report documenting GCMS analysis of sample AE09156 conducted on May 8, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024345
Chain of custody record for GCMS analysis of sample AE10210 on May 20, 2002, including surrogate compound data.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000045682
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated May 3-13 2002.
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NYC-WTC_000045683
Fragmented lab record documenting drip rates, volumes, and pH measurements for environmental samples in May 2002.
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Laboratory report of a GC/MS blank run analyzing volatile organic compounds with results below detection limits in May 2002.
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Laboratory report showing GC/MS calibration verification data for volatile organic compounds with response values in May 2002.
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NYC-WTC_000045702
Laboratory report of GC/MS analysis using reference standards to verify detection of volatile organic compounds in May 2002.
Filed in the same folder