GCMS sample analysis results for AE10699, May 20 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020513\10699.D Vial: 10 Acq On : 13 May 2002 9:25 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.47 ug/1 57630 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

• 1 Anthracene-dlO- 188 C14D10 001719-06-8 72 2 5-Ox^zolecarboxamide, 2-phenyl- 188 C10H8N2O2 039819-42-6 38 3 Phenanthrene-diO 188 C14D10 001517-22-2 38 4 4-F/uoro-6-methyl-2-phenylpyrimi... 188 C11H9FN2 051421-92-2 38 Abundance Scan 4915 (31.958 min): 10699.D (-4903) (-) m/z 188.15 100.00% 188

5000 94 66 158 31.60 31.80 32.00 32.20 I i, 111 130 hadps+dla 256 353 11' i' -HH — upm*mm* m/z 184.20 24.46% •n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79826: Anthracene-d10- 188

5000 1 1 ' 1 1 Tpnu r-r । , । । । ] । i i । । । 31.60 31.80 32.00 32.20 m/ z .94.10 23.41% 66 , 94 16° 17 42 ° J 114132 L I > I I I I I ['ll f11u" I I I II I I I I < I I I I t I I I ‘l I’i I I ‘1‘1‘‘111110"-1—"E‘CTTTTTT‘111111117 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79737: 5-Oxazolecarboxamide, 2-phenyl- 188 116 144 Ti 17IIII Pi । । । । । 31.60 31.80 32.00 32.20 5000 m/z 189.20 15.35% 89 63 39

iz-> .....4r 1 " r '1' i'r'1 r " 11'1 " r '' ■ i' " ' i'r " I " 111111ITTTTT’ l1 " ' I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79827: Phenanthrene-d10 188 31.60 31.80 32.00 32.20 m/ Z 41.00 13.78% 5000

80 160

n/z—> 30 52 , , 100 I I | I I I I |'l rHi [I1! I "FII’l’ |'I " । | 132 . ........ Mus 1 11111"0111’11111101"TTTT7IT i ■11 r i1 " 1 r iAmikia th 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.60 3180 32.00 32.20

10699.D SCAN020507.M Wed May 15 08:36:15 2002 Page 8

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