NYC-WTC_000045707
Laboratory report detailing GC/MS analysis of sample AE10698 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 14 pages
GCMS sample analysis results for AE10699, May 20 2002
Machine-extracted title · confidence 100%Laboratory report detailing GC/MS analysis of sample AE10699 including surrogate recovery data in May 2002.
NYC-WTC_000045721–000045734Folder label: “GCMS X 5/3/02 A 5/13/02”
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NYC 9/11 Public Portal Document
• Data File : C:\MSDCHEM\1\DATA\020513\10699.D vial: 10 Acq On : 13 May 2002 9:25 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 Cyclononasiloxane, octadeca... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T. 32.20 0.44 ug/1 53883 Phenanthrene-dl0 31.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 50 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 36 3 Heptasiloxane, 1,1,3,3,5,5,7,7,9. . . 504 C14H4406Si7 019095-23-9 27 4 Hexasiloxane, 1,1,3,3,5,5,7,7,9,... 430 C12H3805Si6 000995-82-4 23 Abundance Scan 4956 (32.199 min): 10699.D (-4944) (-) m/z 73.05 100.00% 73
5000 5 , Y 147 221 355 429 281 400 I 31.80 32.00 32.20 32.40 32.60 41 ,188,| ............ ‘ I1‘ 1 ' 1 1 1 1 I I 1 ' I 1 I ' ' Y 1 1 1 484 m/z 147.00 19.84% /z->_______ 50 100 150 200 250 350 ' 4Oo' 450 500 300 550 600 650 Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429
355 5000 281 31.80 32.00 32.20 32.40 32.60 m/z 221.10 17.44% 475
Tl/Z-> 1 1 I 1 1 1 ' 1 1 1 50 100 -H 651 150 200 250 300 350 400 450 500 550 600 650 1 1TT । । । । । । । । ( । ।
Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)... 73
147 31.80 32.00 32.20 32.40 32.60 5000 267 m/z 429.00 17.36% 355 429 207
Tl/Z-> | • ‘IB 50 ..II, 100 150 200 L 250 300 1IT 350 400 450 500 550 600 650 Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet... - i 1 1 1 ' 1 1 ' ' ■ i ' ’ 73 31.80 32.00 32.20 32.40 32.60 m/z 355.00 15.70% 5000 207
133 281 355 2.50—— 103 H. 177 1,1 251 . 3251 1 399429 ■ ■ । '1 ■ 1'''111 11 r ■ I I I I I I I / I : I I I I I I I I I ) I 489 ■i"'"11' ।11 I I I I I I I I I I 'I I I I I ..M.... /z-> 100 150 200 250 300 350 400 450 500 550 600 650 31.80 32.00 32.20 32.40 32.60
10699.D SCAN020507.M Wed May 15 08:36:17 2002 Page 9
NYC-WTC_000045733
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