Gas chromatography-mass spectrometry report for sample AE10704 showing detection of unknown compounds and surrogate recovery.
NYC-WTC_000045793–000045810Folder label: “GCMS X 5/3/02 A 5/13/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\DATA\020513\10704.D Vial: 15 Acq On : 14 May 2002 2:23 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 Octasiloxane, 1,1,3,3,5,5,7... Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
34.55 0.30 ug/1 40107 Phenanthrene-dl0 31.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Octasiloxane, /l,1,3,3,5,5,7,7,9, .. . 578 C16H50O7Si8 019095-24-0 45 2 1,1,1,5,7,7,7/-Heptamethyl-3,3-bi . . . 444 C13H40O5Si6 038147-00-1 37 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H36O4Si5 003555-47-3 33 4 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 25 Abundance Scan 5356 (34.549 min): 10704.D (-5343) (-) m/ z 73.10 100.00% 73
5000 147 281 P-4 । mZ ,+-Pu4 221 34.20 34.40 34.60 34.80 327^5 401 429 461 503 41 H+ 115 189 . . . I h i ‘‘ 11 m/z 147.10 34.13% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #27373: Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,1... 73
5000 207 ... 1 । I ' ■ ' ।A"AAA । ' 1 । I 1 . . . I 1 1 ' 1 I 1 34.20 34.40 34.60 34.80 281 m/Z 281.10 28.09% 147 341 45, . 1171,1 177,1 >, 251 _ 313 ( 371 40r11 hi429fn ■ 1 1 1 ' 1 T 1111 | . . I ! | I . . . | 503 563 ' 1 f■ ' ' ' I ' ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #26950: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)... 73
147 34.20 34.40 34.60 34.80
267 m/ Z 221.00 15.16% 5000 355 429 45 207
1 ' i 1 1 1 ' i ■ ' 1,1, m/z-> 50 100 150 250 300 350 400 450 500 550 -— Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime... 73 147 34.20 34.40 34.60 34.80 m/z 207.10 10.32% 281 5000
m/z-> 45 , 1 1Ji 50 100 117 1 ' 1 1 । [ 1-" t -rintrenus f 1" f Ir 1 I"F | I T' । 150 . — 207 249 177 | -11 200 250 310 341 |
300 350 369
| 400 450 । i । ' 1 1 1 । 1 i 500 550 k.... . .... 34.20 34.40 34.60 34.80
10704.D SCAN020507.M Wed May 15 09:01:21 2002 Page 9
NYC-WTC_000045805
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NYC-WTC_000045761
Gas chromatography-mass spectrometry report for sample AE10702 showing detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045707
Laboratory report detailing GC/MS analysis of sample AE10698 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045721
Laboratory report detailing GC/MS analysis of sample AE10699 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045811
Gas chromatography-mass spectrometry report for sample AE10705 showing detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044119
Laboratory report documenting GCMS analysis of sample AE10019 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044227
Laboratory report documenting GCMS analysis of sample AE10067 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044144
Laboratory report documenting GCMS analysis of sample AE10021 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045735
Laboratory report detailing GC/MS analysis of sample AE10700 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044203
Laboratory report documenting GCMS analysis of sample AE10061 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046405
Laboratory report documenting GCMS analysis of sample AE09153 conducted on May 8, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046420
Laboratory report documenting GCMS analysis of sample AE09156 conducted on May 8, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024345
Chain of custody record for GCMS analysis of sample AE10210 on May 20, 2002, including surrogate compound data.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Laboratory report of GC/MS analysis using reference standards to verify detection of volatile organic compounds in May 2002.
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