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GCMS analysis results for sample AE10704, May 20 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report for sample AE10704 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000045793–000045810

Folder label: “GCMS X 5/3/02 A 5/13/02

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Scanned page image, NYC-WTC_000045806
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020513\10704.D Vial: 15 Acq On : 14 May 2002 2:23 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 8 3-Isopropoxy-1,1,1,7,7,7-he... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

36.28 0.39 ug/1 43002 Chrysene-dl2 39.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,7,7,7-hexamet. . . 576 C18H5207Si7 071579-69-6 38 2 1-Monolinoleoylglycerol trimethy... 498 C27H54O4Si2 054284-45-6 28 3 Silane, trimethyl[1-methyl-2-oxo... 218 C9H2202Si2 055255-93-1 27 4 Heptasiloxane, 1,1, y, 3,5,5,7,7,9. . . 504 C14H4406Si7 019095-23-9 17 Abundance Scan 5650 (36.276 min): 10704.D (-5643) (-) m/z 73.05 100.00% 73 h

5000 147 . AAMa AN AA V AA Am a A M____ A 281 355 ”n । i i l l । । k r i rt —i—T 221 43 109 । pul/ot I 'J A/la ". f ' l 1 1401 461 ' 1 1 1 1 ' 1 1 1 1 1 ' I ' ' 36.00 36.20 36.40 36.60 m/z 147.10 40.38% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #26784: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tri... 73

5000 —AA— 147 36.00 36.20 36.40 36.60 m/z 355.10 24.00% JU ... [.. ....I, 347 , ■ , . , ‘ .... .. 561 43 221 281 22— a m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #27370:1 -Monolinoleoylglycerol trimethylsilyl ether 73 .......NA 1 1 1 ' 1 1 1 1 1 207 36.00 36.20 36.40 36.60 5000 147 m/z 280.90 20.98% 34 103

uull . A. । y u J 206. । .355 395 429 ' |’' ' > ■ | . A | A 483 , | , , ' , | ,

m/z-> Abundance 50

73 100 150 200 250 300 350 #26583: Silane, trimethyl[1-methyl-2-oxo-2-(trimethylsilyl... 400 450 500 550 4 A... 1 36.00 36.20 36.40 36.60 m/z 221.00 17.44% 117 147 5000

45 191 218 20, 441 — ----- A—LL miz-> 50 100 150 200 250 300 350 400 450 500 550 36.00 36.20 36.40 36.60

10704 .D SCAN020507 .M Wed May 15 09:01:23 2002 Page 10

NYC-WTC_000045806

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NYC-WTC_000045806Source: NYC Law Department, mirrored locally

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