GCMS sample analysis results for AE10698, May 20 2002

NYC 9/11 Public Portal Document

.Data File : C:\MSDCHEM\1\DATA\020513\10698.D Vial: 9 Acq On : 13 May 2002 8:26 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 3-Isopropoxy-1,1,1,7,7,7-he... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

32.20 0.30 ug/1 29263 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H5207Si7 071579-69-6 17 2 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 10 3 1-Monolinoleoylglycerol trimethy... 498 C27H54O4Si2 054284-45-6 9 4 Trimethylsilyl ether of glycerol 308 C12H3203Si3 006787-10-6 9 Abundance Scan 4956 (32.199 min): 10698.D (-4939) (-) m/ z 73.10 100.00% 73 y

5000 M . ................... ....................... 1 147 188 221 355 429 31.80 32.00 32.20 32.40 32.60 41 । 1 । i r । mpu ■ ■ ■ i ■ ■ ■ ■ i ' 1 ■ ■ i ' r ' ■ n-'-’’' । । । । i-p-i i । । । । । । । । । । । । । । rn/z 147.00 17.63% /z-> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #26784: 3-Isopropoxy-1 ,1,1,7,7,7-hexamethyl-3,5,5-tris(tri... 73

5000 1 ■ i 1 ' 147 31.80 32.00 32.20 32.40 32.60 43 m/z 221.10 16.17% 221 281 327 A1E ..... I.....(327 ....... 415........ 519 561 i । । 1 n ' । 1 1 i 1 1 ■ ■ i ■ ' ■ 1 i ■ f 1 ■ i ■ 1 r ■ i 1 1 1 f I 1 1 1 1 1 1 ' 1 1 I 1 1 1 1 I 11 1 1 I ' 1 m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #26922: Mercaptoacetic acid, bis(trimethylsilyl)- 73 147 31.80 32.00 32.20 32.40 32.60 5000 m/z 355.00 13.30% 221 45 104 193 13. Li L i " 1 r 1 r7 r 14 An FI* ■ * । 1 1 1 i 1 ' ■ ' i 1 ‘ 1 ' i 1 ■ 1 1 i 1 1 ■ 1 i ■ 1 1 ■ i ■ ■ 1 ■ i ' 1 /z-> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #27370:1 -Monolinoleoylglycerol trimethylsilyl ether 73 31.80 32.00 32.20 32.40 32.60 m/Z 188.20 11.95% 207 5000 147

103 281

/z—> 44ll4 177, 249, 1 1325 355 395429 483........ 0 50 100 150 200 250 300 350 400 450 500 550 31.80 32.00 32.20 32.40 32.60

10698.D SCAN020507.M Wed May 15 08:33:47 2002 Page 9

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