GCMS analysis results for sample AE10023, May 2002

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Laboratory report documenting GCMS analysis of sample AE10023 conducted on May 14, 2002, identifying unknown compounds.

NYC-WTC_000044166–000044178

Folder label: “GCMS X 4/26/02 A 5/8/02”

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NYC 9/11 Public Portal Document

- Data File C:\MSDCHEM\1\DATA\020507\10023.D Vial: 22 Acq On 8 May 2002 8:49 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 1,5-Naphthalenedithiole Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.33 ug/1 39265 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,5 -Naphthalenedithiole 192 C10H8S2 1000223-69-5 40 2 3,4-Methylenedioxycinnamic acid 192 C1OH804 002373-80-0 37 3 1H-Indene, 2,3-dihydro-2-methoxy... 224 C16H160 111864-82-5 36 4 5H-Dibenzo[a,d]cyclohepten-5-ol,... 210 C15H140 001210-34-0 33 Abundance / Scan 4768 (31.094 min): 10023.D (-4755) (-) m/z 192.10 100.00% 192

5000

_________ AWA______ 96 146 ti [ iiii ] i । I r J ii । । । r~r

n/z-> TT 40 62 qusstaa 4I?H 0 20 40 60 80 100120140160180200220240260280300320340360380400 334 373 400 TTTT 30.80 31.00 31.20 31.40 m/z 193.10 25.68% Abundance #80950:1,5-Naphthalenedithiole 192

5000 ■ ' i 1 1 ■ ■ i 1 ■ 1 1 1 1 1 1 1 1 1 ' 30.80 31.00 31.20 31.40 128 159 m/z 191.20 21.32% 40 79 1 02 i । r i r । [ i i nt*n */* hrhrr Mri — + T" ' i11111 11'1" r1" i1 ’" । ■1" i1rn ।11111 ■1 • > ।'> 111 1 n/z-> 0 20 40 60 80 100120140160180200220240260280300320340360380400 Abundance #81021: 3,4-Methylenedioxycinnamic acid 192 1.... 4" 30.80 31.00 31.20 31.40 5000 m/ z 96.00 17.73%

63 89 145

Wz-> 4 TTH 39 1 117 1 ’T 164 TTTTT 1 ' ।'1 i" । 0 20 40 60 80 100120140160180200220240260280300320340360380400 i111111111r1" i1111111" 111111111111111111 ‘11

Abundance #81106:1 H-lndene, 2,3-dihydro-2-methoxy-1 -phenyl-, cis- A ' 1 1 1 1 192 30.80 31.00 31.20 31.40 224 m/z 146.00 14.90% 5000

165 91 115 [

n/z—> +26,51,71,4.4413944. TTTT '' ''i1' " i'1" i111'i1"1111" 1 ■ i'11 ‘i""i 1' ......... 1 ................... .... 1 1 1 1 1 1 1 1 ' 1]IIIIJIITT

0 20 40 60 80 100120140160180200 220 240 260280 300 320 340 360 380 400 30.80 31.00 31.20 31.40

10023.D SCAN020507.M Tue May 14 08:45:38 2002 Page 6

NYC-WTC_000044176

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NYC-WTC_000044156

Laboratory report documenting GCMS analysis of sample AE10022 conducted on May 14, 2002, identifying unknown compounds.

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