GCMS analysis results for sample AE08964, May 7, 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020424\08964.D Vial: 15 Acq On : 24 Apr 2002 11:37 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 1,5-Naphthalenedithiole Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.30 ug/1 535985 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 45 2 Thiocyanic acid, 2-benzothiazoly. . . 192 C8H4N2S2 006011-99-0 42 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 42 4 1^2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 1000196-69-5 42 Abundance Scan 4768 (31.094 min): 08964.D (-4757) (-) m/z 192.10 100.00% 192

5000 40 \ T ’rI T

iz-> * l “ “ i' ‘ 51 TT zp..42.1,122, 49 100 . 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 200 — m/z 30.80 31.00 31.20 31.40 RW—OWWWV 40.10 25.74% Abundance #80950:1,5-Naphthalenedithiole 1512

5000 T 30.80 31.00 31.20 31.40 115 128 159 m/z 96.00 15.51% 40 57 69 79 96 147 rr 11111. ... . 11 177 Tp-n-rp-r TTITT niz-> 20 30 40 50 60 70 80 90 100110 120130 140150160 170 180190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 1912 ‘ I‘ ‘ i j » • 30.80 31.00 31.20 31.40 5000 m/z 191.00 14.46%

mnmmmmmhmmdmtmmmg 45 1,90 108 122 134 148 160. 1 I miz—> Abundance :20 30 40 50 60 70 80 90 100 110 120 130140150160170180 190 200 #125842: Phenanthrene, 2-methyl- 1912 m 30,80 31.00 31.20 31.40 m/z 193.10 13.78% 5000

96 . /z—> 27 39 51 63 mWTPWNTTTTTTTT*TTTTT)*IWPTTTWmTTTTTTTHTT 82 ll 115 126 139 152 165 176 20 30 40 50 60 70 80 90 100110120 130 140150160170180 190 200 JL 30.80 31.00 31.20 31.40

08964.D SCAN020424.M Thu May 02 14:53:03 2002 Page 6

NYC-WTC_000049631