GCMS analysis results for sample AE08969, May 7, 2002

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'Data File : C:\MSDCHEM\l\DATA\020424\08969.D Vial: 17 Acq On : 25 Apr 2002 1:35 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************* * *********************** Peak Number 7 Naphthalene, 1,7-dimethoxy- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.30 ug/1 555417 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 45 2 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 42 3 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 38 4 Anthracene-dlO- 188 C14D10 001719-06-8 38 Abundance Scan 4915 (31.958 min): 08969.D (-4904) (-) m/z 188.20 100.00% 188

5000 - 80 94 158 31 60 31.80 32.00 32.20 42 54 66 ,i TPWPTTPTTTINTTTTTTTTTTTNT . 128 11 ■ “ mm m/z 189.20 19.37% n/z-> 2) 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79804: Naphthalene, 1,7-dimethoxy- 173 188

i T | t I t l' | 1 ! I J pT 5000 1I 3160 31.80 32.00 32.20 102 115 145 m/z 94.00 15.62% 51 63 75 94 130 TRmRmmTpHpH TPTTHT . i.... ।...158 11" ‘111 1 ।• ■ ■ ■ mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 FT I —r * 31.60 31.80 32.00 32.20 5000 m/z 80.10 9.91% 143 51 64 76 89 102 115।130 |, 158 170 mptptp > ।।।. 111 p ... ।. ri. p m ।.. A ..., 11, >, ।. it. ।...TH rT ... Me > | r > > I j > > ■ i h ■ 111 n’ll i > fm-r nfz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79714: Pentacycfo[8.4.0.0(3,7).0(4,14).0(6,11))tetradecane ___________ ____________ 1 188 J j 1 » /T ] » i : i j J 1 "T"} I 188 31.60 31.80 32.00 32.20 m/z 184.10 9.75% 5000 79 91 117 131- 145 159 173 106 . 27 • i “ "i 41 55 T - —lyrlp— Hasyand n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

08969.D SCAN020424.M Thu May 02 15:00:40 2002 Page 9

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