GCMS analysis results for sample AE08969, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08969 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049644–000049657

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

•Data File : C:\MSDCHEM\1\DATA\020424\08969.D Vial: 17 Acq On : 25 Apr 2002 1:35 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 9H-Fluorene, 9-ethylidene- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.08 0.31 ug/1 573955 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 9H-Fluorene, 9-ethylidene- 192 C15H12 007151-64-6 53 2 Bitoscanate 192 C8H4N2S2 004044-65-9 52 3 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 45 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 45 Abundance Scan 4766 (31.082 min): 08969.D (-4756) (-) m/z 192.10 100.00% 1:2

5000

40 64 82 % 120 146 160 j,, 11 j.... |.... |.... 1.. 1. |.... |.... 1, 1.11.... | h ., |. I'l.!.... 11.11111111111111 1'1111111 fri t | | 111111111 | 11111 30.80 31.00 31.20 31.40 m/z 191.00 16.68% miz-> 0 1020304050607080 90100110120130140150160170180190200 Abundance #81028: 9H-Fluorene, 9-ethylidene- 192

5000 165 30.80 31.00 31.20 31.40 m/z 96.20 13.14% 83 99 .................. 41....................... I.............. .............. I ।।11।।।।11...।,, I..t...11....11।t.. ‘ ‘I’’ mlz-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #125827: Bitoscanate 1912

30.80 31.00 31.20 31.40 5000- m/z 193.10 11.42% 134 50 90 160 63 TO

niz-> ,4..,14..281. +4+lh**+*192116 . . 0 10 2030405060 70 8090 100110120130140150160170180190200 148 ’r t n h I'll 111i'I'Ii |'i i ri 11111 |'ti‘i 11 h ■ i' "• i

Abundance #80862:1,2-Phenylene diisothiocyanate 1 ■ i ' 1 ■ 1 I ■ ■ 192 30.80 31.00 31.20 31.40 m/z 146.00 11.27% 64 5000 I 90 134 39 50 75

n/z—> 4 18.29+— . ++++ , । 107 148 160 l’ iT . fl i. 11 ■. I. j l.. 11 ’ ■ ।... t!| ........................... ■ i ■"■ i ‘1 . 122, | ।।। it ।, 0 10 2030405060 70 8090 100110120130140150160170180190200 30.80 31.00 31.20 31.40

08969.D SCAN020424.M Thu May 02 15:00:40 2002 Page 8

NYC-WTC_000049655

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GCMS analysis results for sample AE08960, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049571

Laboratory report documenting GCMS analysis of sample AE08960 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998