GCMS analysis results for sample AE08965, May 7, 2002

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Data File : C:\MSDCHEM\1\DATA\020424\08965.D Vial: 16 Acq On : 25 Apr 2002 12:36 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.28 ug/1 537001 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 56 2 Anthracene-dlO- 188 C14D10 001719-06-8 47 3 Pentacyclo[7.3.1.1.(4,12).0(2,7).. . 188 C14H20 1000215-61-8 45 4 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 9 Abundance Scan 4915 (31.958 min): 08965.D (-4905) (-) m/z 188.20 100.00% 188

5000

80 94 31.60 31.80 32.00 32.20

m/z-> 40 51 66 , TITTTmTPTTTTTTTTTTTTNTTT Ik ' i “ *' I 136148.1%....li p-TTT 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 m/z 189.10 19.72% Abundance #79827: Phenanthrene-d10 188

—, 4 5000 31.60 31.80 32.00 32.20 80 m/z 80.20 17.66% 94 160 30 42 52 IWWITTTTTTTTTHTTTH 66 . 44.108,118.132.146417917. miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 118 • Y. • r | T-T P > I I I I I I I I I r

3160 31.80 32.00 32.20 5000 m/z 184.20 16.76%

80 94 160 | 17 30 42 52 00 . . 108118 132 146 jj 170179.1,। T TPpmmmmmmmammmmmmppmpt" tttt iz—> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 Abundance #79715: Pentacyclo(7.3.1.1.(4,12).0(2,7).0(6,11)]tetracleca... TI ------ 188 31.60 31.80 32.00 32.20 m/z 94.20 15.25%

5000 79 91 55 67

xwXxxzx 131

n/z—> .. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 173 •i ■ r' ‘ | 4 "I ■ 1 ri 0 31,60 31.80 32.00 32.20

08965.D SCAN020424.M Thu May 02 14:58:50 2002 Page 5

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