GCMS analysis results for sample AE08965, May 7, 2002

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Data File : C:\MSDCHEM\1\DATA\020424\08965.D Vial: 16 Acq On : 25 Apr 2002 12:36 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 *********************************** * * ******************************** Peak Number 2 1,5-Naphthalenedithiole Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.10 0.29 ug/1 542934 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 45 2 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 42 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 42 4 Phenanthrene , 1-methyl- 192 C15H12 000832-69-9 42 Abundance Scan 4768 (31.094 min): 08965.D (-4759) (-) m/z 192.05 100.00% 192

5000 40 96 t-r-j-r-T T-r-p-r 82 146 49 70 106 122 160 I 30.80 31.00 31.20 31.40 I ll'j i . I > I ll ■ | 111'11 | i rl i 11 n I!i 11 ■ I 11 I r r - m/z 40.10 41.41% m/z-> ‘1’11171 ha 20 30 40 50 60 70 80 90 100 110120 130140150160 170180190 200 Abundance #80950:1,5-Naphthalenedithiole 19 2

5000 159 30.80 31.00 31.20 31.40 115 128 m/z 96.10 22.60% 40 57 69 79 96 147 177 ------- 'l l I'll 1111 > 11.TTpmgr ■ ■i“ miz-> 20 30 40 50 60 70 80 90 100110120130140150 160 170 180190 200 Abundance #81041: Phenanthrene, 3-methyl- 192 T T T 30.80 31.00 31.20 31.40 5000 m/z 191.10 19.82%

96 iff? 63 27 82 39 ]| 51115 126 139 152 165 176 TWTTTTTTTTht 1tTTTTT miz-> 2030405060 70 8090 100110120130140150160170180190200 Abundance #125842: Phenanthrene, 2-methyl- T T l • • • • j • • 19 2 30.80 31.00 31.20 31.40 m/z 193.10 17.60%

5000

96 27 39 51 63 82 l 115 ■ TVE 152 165 176 । Trr 139 asttassyeHapashngandT 126 mogov uIganaapem T . m 111 i'| n ■ ■ 111 ii । i'i 11| । n । plh rh‘ rl i iz—> 20 30 40 50 60 70 80 90 100 110 120 130140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

08965.D SCAN020424.M Thu May 02 14:58:48 2002 Page 4

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