GCMS analysis results for sample AE08963, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08963 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049609–000049621

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

‘Data File : C:\MSDCHEM\1\DATA\020424\08963.D Vial: 14 Acq On : 24 Apr 2002 10:39 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library . : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Phenanthrene, 9-methyl- . Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.31 ug/1 604426 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 64 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 59 3 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 59 4 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 40 Abundance Scan 4768 (31.094 min): 08963.D (-4759) (-) m/z 192.05 100.00% 192

40 5000

96 146 160 82 30.80 31.00 31.20 31.40 . 54 66 118 Tp-n-q-m-r I'* > > )• ।' 1111 11111 Tmmmp pHmmm ‘ I m/z 40.10 51.53% miz-> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 152

5000 30.80 31.00 31.20 31.40 m/z 191.10 27.79% 96 4Pr 29 39 51 63 74 83 115 126 139 152 ? 176 . | . ।.... ।... r, >.., p 11., Th , ।. ri. l’i rh) rM ‘ j ■ ■ 11 pw 111 ■ i < 111 > i'| i > p-i 1 11 i’ri 11 r rl 11 r’1 1 ‘ I “ n/z-> 20 30 40 50 60 70 80 90 100110120130140 150160170180190 200 Abundance #80950:1,5-Naphthalenedithiole 192 .. A............ 30.80 31.00 31.20 31.40 5000 m/z 96.10 18.84% 159 A) 115 128 40 57 69 79 96 147 < । * * * 11 »rpr" * i' ----- * M । I'ri /prrtrer rl 111 lrp 11 rh 111 Ar 11> nmns p 177 । r 111 riII 1111 miz-> 20 30 40 50 60 70 80 90 100110120 130140150160170 180190 200 Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- TBBBnnn 1 1 i • ■ 1 ‘ i 1(2 30.80 31.00 31.20 31.40 164 m/z 146.10 15.58% 5000 99 115 47 77 177 67 125 146 127.39, ,157 , 1'1 +87. plv, Pl 17l4++4155, 4 HH 4+ n/z—> 20 30 40 50 60 70 80 90 100110120130140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

08963.D SCAN020424.M Thu May 02 14:52:42 2002 Page 7

NYC-WTC_000049619

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GCMS analysis results for sample AE08960, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049571

Laboratory report documenting GCMS analysis of sample AE08960 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998