GCMS analysis results for sample AE10705, May 20 2002

NYC 9/11 Public Portal Document

• Data File : C:\MSDCHEM\1\DATA\020513\10705.D Vial: 16 Acq On : 14 May 2002 3:23 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Phenanthrene, 1-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.33 ug/1 40391 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 53 2 2,5-Dihydrophosphole, 3-methyl-l. . . 192 C11H130P 1000196-97-5 53 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 49 Abundance Scan 4767 (31.088 min): 10705.D (-4755) (-) m/z 192.20 100.00% 102

5000

22 84 146 423..11119 rjiiii। ii .. i ky t r 1 , 512 30.80 31.00 31.20 31.40 m/ z 191.00 28.57% m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #125856: Phenanthrene, 1-methyl- 102

5000 A AA 30.80 31.00 31.20 31.40 m/z 146.10 17.53% 96 PE 39 63 .1139 _ /z—> 50 100 150 200 250 300 350 400 450 500 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1-phenyl- . 164 192 30.80 31.00 31.20 31.40 5000 99 m/z 192.90 16.96% 47 125 .. I. > ।. । J .L.ii I l — ■ 1 " I 1 L' i ■ ' 1 ■ i 1 L' ■ i ' ■ ■ ■ i ■ 1 ‘ 1 i 1 1 ■ 1 i ' m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #81033: Phenanthrene, 9-methyl- AA .... ■ ■ । 1 1 1 1 । ' 1 1 1 i 1 1 1 1 । 1 1 102 30.80 31.00 31.20 31.40 m/z 84.00 14.16% 5000

_ 39 63 96 J 139 165 J. | ................................ ' ' I ' 1 ' ' i 1 1 ' 1 1 ' ' 1 ' i • ■ • • । ■ ■ . ■ । • i । • । । ■ । । < ' । । > । ■ । । । । 1 ' i 1 ' 11 i 11 ■ i ■ ■ /z--> 50 100 150 200 250 300 350 400 450 500 30.80 31.00 31.20 31.40

10705 .D SCAN020507 .M Wed May 15 09:03:21 2002 Page 6

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