Gas chromatography-mass spectrometry report for sample AE10705 showing detection of unknown compounds and surrogate recovery.
NYC-WTC_000045811–000045823Folder label: “GCMS X 5/3/02 A 5/13/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
‘ Data File : C:\MSDCHEM\1\DATA\020513\10705.D Vial: 16 Acq On : 14 May 2002 3:23 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1
Peak Number 3 Benzoic acid, 2,4-bis[(trim... Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T. 28.36 0.40 ug/1 49205 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4Si3 010586-16-0 32 2 N-(Trifluo/oacetyl)-0,0',0"-tri. . . 481 C19H34F3NO4Si3 1000072-26-3 23 3 Phenethylamine , N-methyl - . beta. , . . . 399 C18H37NO3Si3 010538-85-9 23 4 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 23 Abundance Scan 4303 (28.362 min): 10705.D (-4291) (-) m/z 73.10 100.00% 73 N
5000 147 221 355 J \..... i | > r2 i ] AA 11 i PA- 1-—A—i—।—r
m/z-> 43 ■ । ,i 1 50 1 1 117 1 I 1 '■ 100 150 200 187 250 282 313 ----fr 1* 300 350 1. 400 401
450 28.00 28.20 28.40 28.60 m/z 147.10 46.24% Abundance #115312: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trim... 70
5000 355 —A.h., 28.00 28.20 28.40 28.60 ' ■ I ' ' ' ' I 1
45 m/z 355.10 43.98% 16 , . ■ ■ i 'i 1 1 " f |', » trhin n 105 133,163 193 "i 251 rj 4 223 /W 281 । । ।321 . । - -* 1 , m/z-> 50 100 150 200 250 300 350 400 450 Abundance #27960: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)n... 73 ................. f ' I ' ' 1 ■ 1 1 1 1 1 I ' ' 1 ' 1 1 1 1 1 I r 355 28.00 28.20 28.40 28.60 5000 m/z 221.10 34.63%
45 ] 120 147170193 236 265 377 481 ■ • i ■ • r ■ /z-> 50 100 150 200 250 300 350 400 450 Abundance #115313: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... ' i ■ 1 ' 1 i 1 1 73 28.00 28.20 28.40 28.60 m/ Z 74.00 18.83%
5000 355
m/z-> XI 50 100 116 147 150 193 22Q 200 267 294 250 300 350 384 400 450 .. .... 1.4...... 28.00 28.20 28.40 28.60
10705.D SCAN020507.M Wed May 15 09:03:19 2002 Page 5
NYC-WTC_000045819
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NYC-WTC_000045721
Laboratory report detailing GC/MS analysis of sample AE10699 including surrogate recovery data in May 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045707
Laboratory report detailing GC/MS analysis of sample AE10698 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044119
Laboratory report documenting GCMS analysis of sample AE10019 conducted on May 14, 2002, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044215
Laboratory report documenting GCMS analysis of sample AE10066 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044166
Laboratory report documenting GCMS analysis of sample AE10023 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045793
Gas chromatography-mass spectrometry report for sample AE10704 showing detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045761
Gas chromatography-mass spectrometry report for sample AE10702 showing detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044227
Laboratory report documenting GCMS analysis of sample AE10067 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044132
Laboratory report documenting GCMS analysis of sample AE10020 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044179
Laboratory report documenting GCMS analysis of sample AE10024 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044203
Laboratory report documenting GCMS analysis of sample AE10061 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044144
Laboratory report documenting GCMS analysis of sample AE10021 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000045682
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NYC-WTC_000045683
Fragmented lab record documenting drip rates, volumes, and pH measurements for environmental samples in May 2002.
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Laboratory report of a GC/MS blank run analyzing volatile organic compounds with results below detection limits in May 2002.
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NYC-WTC_000045698
Laboratory report showing GC/MS calibration verification data for volatile organic compounds with response values in May 2002.
Filed in the same folder
NYC-WTC_000045702
Laboratory report of GC/MS analysis using reference standards to verify detection of volatile organic compounds in May 2002.
Filed in the same folder