GCMS analysis results for sample AE10066, May 2002

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Laboratory report documenting GCMS analysis of sample AE10066 conducted on May 14, 2002, including surrogate recovery data.

NYC-WTC_000044215–000044226

Folder label: “GCMS X 4/26/02 A 5/8/02”

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\020507\10066.D Vial: 26 Acq On 8 May 2002 12 :45 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Phenanthrene, 9-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.38 ug/1 38274 Phenanthrene-dl0 31.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 53 3 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 53 4 9H-Fluorene, 9-ethylidene- 192 C15H12 007151-64-6 50 Abundance / Scan 4767 (31.088 min): 10066.D (-4755) (-) m/z 192.10 100.00% 192

5000

■ ' i ' 1 1 ‘ i 1 1 1 ■ i r ' 1 1 i 1 ' 96 146 30.80 31.00 31.20 31.40 42 66 I. | 118 | 1,64 |i 306 366 m/z 193.00 TT’ ' i111' i'1' " i11 " i '' ■ 11 ■ ■ ■ -1 ■ ■ ■ > । । ‘ ■ I Ti | i i > I | I | i i | > i i i | i > i r | i i i i | | i i j | | | i | | I | I PF’r"r 14.96% /z-> 0 20 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 1 I ■ ■ ' ' i 1 1 30.80 31.00 31.20 31.40 m/ Z 190.90 12.94% 96 165 | 39 63 115 139 j , J •| > C" 1* iit H| ■ ' 0 1****)’ 1 ' Tfi it ’I"8111’0011101111101000111-0TTB-T017 ’—7—r /z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #125842: Phenanthrene, 2-methyl- 192 I...... | li..... 1 1 r1 1 1 1 । 1 1 30.80 31.00 31.20 31.40 5000 m/z 146.10 12.42%

96 , V 39 63 , j 115 139 195, 11.... 1111 11. r. <1^ wTit 11 । > । > 11 < ।.‘| । i*i 11 Ti । fyuT r "' i11" i " " r 1" i " 11 r " 1 r ■" i" " i' ................... )..................... m/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #80862:1,2-Phenylene diisothiocyanate 192 30.80 31.00 31.20 31.40 m/ z 96.00 12.04% 64 5000

90 134

/z—> Ti 0 18.1444 107 I 160 dnti l [Jl I fl [ I 11 11 I 111111

20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ' i" " r1" i" " i " ■' r " ‘ i " " r 1" r 1" i" AL 30.80 31.00 31.20 31.40

10066.D SCAN020507 .M Tue May 14 08:47:04 2002 Page 5

NYC-WTC_000044224

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