GCMS sample analysis results for AE10698, May 20 2002

NYC 9/11 Public Portal Document

‘Data File : C:\MSDCHEM\1\DATA\020513\10698.D Vial : 9 Acq On : 13 May 2002 8:26 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 * ******************************************************************** Peak Number 6 Phenanthrene-diO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.39 ug/1 39096 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-d10 001517-22-2 91 188 C14D10 2 Anthracene-dl0- 001719-06-8 90 188 C14D10 3 Perftacyclo[7.3.1.1.(4,12).0(2,7)... 1000215-61-8 53 188 C14H20 4 Antipyrine '188 C11H12N2O 000060-80-0 43 Abundance Scan 4914 (31.952 min): 10698.D (-4906) (-) m/z 188.20 100.00% 188

5000

80 158 1 1 i 1 1 'T i 1 1 1 '"i1"1 । । 1 31.60 31.80 32.00 32.20 ..... 43.64 1441124 '1' i11 ‘' i11 ‘11 ‘ ■ । ■ ■ ■ ■ t ■ ■ । 347 । > ■ ■ ■ । - ■ ■ ■ 11 ■ ■ ■ । < 1111 ■ > ■ 11 ■ 1 ■ ■ m/ z 80.00 20.85% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79827: Phenanthrene-d10 188

5000 * 31.60 31.80 32.00 32.20 m/z 184.00 16.45% 80 160 30 52 100 m/z-> । । | m i i |‘i i l‘i |l ‘i i HTth pri rrr 20 40 60 132,14... . < । । । । । । । । r! ■ i ■ [' i

80 100 120 140 160 180 200 220 240 260 280 300 320 340 i111' r r'' 111'11 ■1 ■1 r '

Abundance #79826: Anthracene-d 10- 108 ‘II/‘I1*‘*IIIIII 1" । । । > 31.60 31.80 32.00 32.20 5000 m/ z .94.10 14.72%

RR 94 160

1742.661114 132_ । । । ' । i i । i i । । । । rrr J ill i | II li । I ill । it । I y । i < । | J 1‘1‘771111111010T011711TTTT"——I1BIII"T m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79715: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... 1 ' | 1 ■ 1 ■ I'' ' ■ T | 1 ■ ■ I | I I > I | > 188 31.60 31.80 32.00 32.20 m/z 189.20 14.19%

5000 91 55 131 159 T I | / . I I — I I I I—|—I—I—I—|—|—T

....... 1,1,1 .1 > i ■ ■1 > i ■ ■ > 11 ■ + "IIrr . > । m ‘I’’’ ‘T’’’’ । <>> i । । । । । । । i । । । m n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.60 31.80 32.00 32.20

10698.D SCAN020507.M Wed May 15 08:33:47 2002 Page 8

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